The a-GaN films were successfully grown on the r-sapphire substrate by MOCVD method. The structure of V-defects was investigated by AFM and SEM. The dependence of V-defects density on growth temperature of a-GaN film at a constant hydrogen flow through a TEG source was studied. The influence of V/III ratio on V-defects structure was investigated. Methods of V-defects density minimisation were purposed.
Investigation of the effect of crystal defects on nonpolar a-GaN films grown by metalorganic chemical vapor deposition on r-sapphire substrates is presented. Samples were grown at different temperatures and the same V/III ratio. High-temperature nucleation in combination with low-temperature GaN buffer layer growth was used to achieve a smooth morphology and “mirror” surface. The macrostructures of the defects were investigated using a scanning electron microscope. Defect concentration via dislocation type correlation was analyzed by diffractometry investigation. Structural quality was investigated via x-ray diffraction. The correlation between the densities of mixed threading dislocations and V-defects was determined. It was detected that the origin of V-defects on the a-plane and c-plane was the same despite having completely different geometries and structures. We also investigated the dependence of V-defect density on a-GaN film growth temperature at a constant hydrogen flow through a triethylgallium source, and we also investigated how the V/III ratio influenced the V-defect structure. Optimum growth parameters for defect concentration reduction were determined.
The AlGaInAs structure was successfully grown on the InP substrate by MOCVD method. The active region was studied by Auger spectroscopy. The thicknesses and compositions of the quantum wells did not coincide with the theoretical ones. The mathematical model which correlate with investigation results is proposed.
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