New clinoptilolite‐based conductometric sensors were developed and optimized for selective detection of ammonium in the buffered aqueous solutions. The sensors’ selective elements were prepared by subsequent drop‐casting of zeolite and Nafion on the gold electrode surface. Electrochemical impedance spectroscopy and differential conductometry were used to investigate the sensor performance. As determined in the phosphate buffer solution, the detection limit of the sensors was 30 μM and the linear range 0–1.5 mM. The developed sensors were featured with a simple preparation procedure, high selectivity to normalNnormalH4+
, and storage stability for not less than 126 days.
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