Vitamin E and selenium supplementation at the given level can inhibit CCl(4)-induced activation and proliferation of HSCs and promote the apoptosis of activated HSCs in acute damage phase. Vitamin E and selenium can also effectively decrease the degree of hepatic fibrosis and promote the recovery process.
In this paper, orthogonal experiment design method was applied to determine the optimum condition for indium leaching from indium-poor zinc residue in HCl solution. Taking the results of range analysis and the situation of industrial production into consideration, the optimum conditions for conventional leaching are: reaction temperature 70°C, concentration of HCl 6 mol/L, leaching time 1.0 h, and ratio of liquid to solid 8:1. Under the optimum conditions, ultrasonic was used to enhance the leaching process. Compared with the conventional leaching process, this new process can provide better indium recovery, shorter leaching time, and faster leaching rate. The indium extraction of indium-poor zinc residue with ultrasonic treatment is up to 96 %, which is 31.0 % higher than that without ultrasonic treatment. In addition, the normal agitation improves the diffusion of solution in the ultrasonically enhanced leaching experiment.
This study was concerned with the effects of mechanical activation (MA) on structural characterization for neutral leach residue of zinc calcine (NLR) and kinetics of indium extraction from NLR in sulphuric acid. The X-ray diffraction (XRD) analysis showed that MA caused the decrease in crystalline phase and increase in lattice distortion. The activation time, reaction temperature and H2SO4concentration had positive effect on indium extraction from NLR. The activation energies of the unactivated, milled for 30 and 60 min NLR samples calculated for indium extraction were 39.3, 32.1, and 30.4 kJ/mol, respectively, which indicated that MA increased the leaching kinetics of indium extraction from NLR. The empirical orders of the unactivated, activated for 30 and 60 min samples for extracting indium with respect to H2SO4concentration were 0.52, 0.51, and 0.51, respectively.
The impact of HPD722 macroporous resin on the dynamic adsorption and desorption of flavonoids in Emilia Sonchifolia extract is studied. The diameter-height ratio of macroporous resin column is 1:10; the mass concentration of the sample solution is selected to be 50.00 mg•mL-1; while the sample flow rate is 3.00mL min-1; upon dynamic absorption for once, the absorption rate reaches 81.11%; with adoption of 50mL ethanol at a volume ratio of 60% as the desorption agent, the desorption flow rate comes to 3.00mL•min-1; and the desorption rate of flavonoids attains 85.26%. Under optimal conditions, the content of flavonoids increases from 6.05% to 32.65% upon purification by HPD722 macroporous resin.
Single factor experiments and orthogonal experiments were successively carried out to optimize the water extraction technology of flavonoids in Thlaspi arvense Linn. Results showed that the influential order of factors was extraction times >solid-liquid ratio >extraction time. The optimum conditions were adding 16 times amount of water, extracting 3 times and every time with 4 hours. Under these conditions, the yield of flavonoids from Thlaspi arvense Linn was 1.17%.
The impact of HPD722 macroporous resin on the dynamic adsorption and desorption of flavonoids in Thlaspi arvense Linn extract is studied. Obtained optimal conditions:the mass concentration of the sample solution is selected to be 4 mg•mL-1; while the flow rate of sampling is 1.30mL min-1; pH value is 4;50mL ethanol at a volume ratio of 70% is adopted as the desorption agent;the desorption flow rate reaches 3.47 mL•min-1. Under these conditions, the content of flavonoids increases from 5.09% to 21.91% upon purification by HPD722 macroporous resin.
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