ABSTRAKE glass ber dental adalah ber yang sering digunakan di kedokteran gigi. Ketersediaan E glass ber di Indonesia masih sangat terbatas. Berbagai jenis bahan glass ber non dental banyak ditemukan dipasaran sebagai material engeenering dengan harga yang relatif murah sehingga diharapkan dapat digunakan sebagai alternatif pengganti E glass ber dental. Komposisi glass ber non dental hampir sama dengan E glass ber dental. Komposisi berpengaruh terhadap sifat mekanis dan sifat-sifat kimia ber. Komposisi glass ber seperti Na 2 O dan K 2 O akan meningkatkan ketahanan terhadapap air. Tujuan dari penelitian ini adalah mengetahui pengaruh komposisi glass ber non dental terhadap kelarutan komponen. Bahan yang digunakan dalam penelitian ini adalah E glass ber dental (Fiber-splint, Polydentia SA, Switzerland), glass ber non dental komposisi A (LT, China), komposisi B (CMAX, China), komposisi C (HJ, China), owable komposit (CharmFill Flow, Denkist, Korea) dan silane coupling agent (Monobond S, Ivoclar Vivadent, Liechtenstein). Subjek dibagi dalam 4 kelompok untuk dilakukan uji kelarutan berdasarkan ISO 4049. Hasil yang diperoleh dianalisis menggunakan ANAVA satu jalur (α = 0,05). Hasil penelitian menunjukkan rerata kelarutan komponen (%) yang terendah pada kelompok E-glass ber dental (0,476±0,03) dan hasil tertinggi pada glass ber non dental C (0,600±0,01). Hasil uji Anava satu jalur menunjukkan perbedaan yang bermakna antara komposisi ber pada kelarutan komponen (p<0,05). Kesimpulan penelitian adalah komposisi Na 2 O dan K 2 O serta CaO dan MgO yang rendah dapat menurunkan sifat kelarutan komponen dari ber reinforced composites.Kata kunci: glass ber non dental, kelarutan komponen, komposisi ber ABSTRACT: The effect of composition glass ber non dental on water solubility of ber reinforced composites. E glass ber dental is one of the most used dental bers in several applications in the dental eld. However, the available of E glass ber dental in Indonesia is very limited. A variety of types of non-dental glass ber material is easily found as the materials engineering. The purpose of the study was to evaluate the effect of composition non dental glass ber on the component solubility of FRC. The materials used in the research was E glass ber dental (Fiber splint, Polydentia SA, Switzerland), composition A non-dental glass ber (LT, China), composition B (CMAX, China), composition C (HJ, China), owable composite (Charm ll Flow, Denkist, Korea) and silane coupling agent (Monobond S, Ivoclair Vivadent, Liechtenstein). The subject was divided into 4 groups. Component solubility test was based on the ISO 4049. The result was then analyzed with one way ANOVA (α=0,05). The result of the research showed that on the average percentage of the solubility (%), the lowest was on the group of E glass ber dental (0.476±0.03) and the highest was on the non dental glass ber C (0.600±0.01). The result of the one way ANOVA test showed a signi cant difference between the composi...
Hydroxyapatite (HA) has been deposited on silica (SiO2) particles to produce HA-SiO2 composite that will be used as the powder component of calcium phosphate cement. HA was expected to be on the composite surface to maintain its bioactivity. SiO2 was made by the sol-gel method, in which silicate solution was extracted from rice husk ash with NaOH solution. Deposition of HA on SiO2 was carried out by wet chemical deposition method at various Ca/Si molar ratio (in a range of 5–25) followed by calcination at 600 °C for 2 h. Results showed that HA was successfully deposited on SiO2 particles. The cell parameters of the HA crystals were slightly distorted by the presence of SiO2 and HA in the composite had a bigger cell volume than pure HA. The crystallite size of HA in the composites increased with the increase of the Ca/Si ratio but the values were smaller than pure HA. SiO2 acted as a morphology directing agent. At low Ca/Si ratio, the HA-SiO2 particles were in a form of short rod-like particles with sizes of < 50 nm, while at high Ca/Si ratio, a mixture of short and long rod-like particles with the size of < 100 nm was obtained. The zeta potential of composites was almost similar to pure HA. These properties indicated that HA-SiO2 composites support the bioactivity of injectable calcium phosphate cement.
ABSTRAKResin akrilik merupakan bahan yang sering digunakan dalam pembuatan basis gigi tiruan. Kelemahan resin akrilik adalah mudah patah. Salah satu cara untuk mengatasi masalah tersebut adalah dengan menambahkan polyethylene (PE) atau glass fiber. Tujuan dari penelitian ini untuk mengetahui pengaruh jenis dan volumetrik fiber terhadap kekuatan transversal reparasi plat resin akrilik. Penelitian ini menggunakan dua puluh lima plat resin akrilik kuring panas berukuran 65 x 10 x 2,5 mm. Subjek dipreparasi untuk membuat jarak 3 mm dan sudut bevel 45 o . Subjek dibagi menjadi 5 kelompok, masingmasing kelompok terdiri dari 5 subjek. Kelompok 1 (kontrol) tanpa penambahan fiber, kelompok II dengan penambahan 3,7% v/v PE fiber, kelompok III dengan penambahan 7,4% v/v PE fiber, kelompok IV dengan penambahan 3,7% v/v E-glass fiber, dan kelompok V dengan penambahan 7,4% v/v E-glass fiber. Seluruh plat direndam dalam air destilasi selama satu hari pada suhu 37 o C. Pengujian kekuatan transversal plat resin akrilik dengan menggunakan Universal Testing Machine dan data yang didapat dianalisis menggunakan ANAVA dua jalur dengan tingkat kepercayaan 95%. Rerata kekuatan transversal (MPa) reparasi plat resin akrilik yang diperkuat fiber: 3,7% v/v PE fiber (67,77±3,34); 7,4% v/v PE fiber (80,37±8,42); 3,7% v/v E-glass fiber (96,72±5,43); 7,4% v/v E-glass fiber (109,44±4,98); sedangkan reparasi plat resin yang tidak diperkuat fiber menghasilkan kekuatan transversal 56,27±4,7 MPa. Hasil analisis menggunakan ANAVA dua jalur menunjukkan variabel jenis dan volumetrik fiber memberikan pengaruh signifikan (p<0,05), sedangkan interaksi antara jenis dan volumetrik fiber tidak berpengaruh signifikan (p>0,05). Uji post hoc Tukey menunjukkan perbedaan signifikan (p<0,05) untuk seluruh kelompok perlakuan. Penambahan E-glass fiber dalam reparasi plat resin akrilik mampu meningkatkan kekuatan transversal lebih tinggi dibandingkan dengan menggunakan PE fiber. Peningkatan volumetrik fiber dapat meningkatkan kekuatan transversal reparasi plat resin akrilik. Maj Ked Gi Ind. Juni 2015; 1(1): hal 102-108 Kata Kunci: E-glass fiber, polyethylene fiber, volumetrik fiber, kekuatan transversal, reparasi akrilik reinforcement, group II reinforced with 3.7% v/v PE fiber, group III reinforced with 7.4% v/v PE fiber, 7% v/v PE fiber was (67.77±3.34); 7.4% v/v PE fiber (80.37±8.42); ABSTRACT: Effect Of Type And Volumetric Fiber On Transverse Strength Of Acrylic Resin Plate Repair. Acrylic resin is the most common denture base material. A disadvantage of acrylic resin is that it is easily fractured. One way to resolve this problem is by adding polyethylene (PE) or glass fibers. The purpose of this research is to find out about the effect of type and volumetric fiber on transverse strength of acrylic resin plate repaired. The experiment involved twenty five plates of heat cured acrylic with the dimensions of 65 x 10 x 2.5 mm. The speciments were prepared to create a 3 mm gap and 45° bevel. The subjects were divided into 5 groups; each group consisted of 5. Gro...
Perawatan di kedokteran gigi mulai menggunakan material fiber reinforced composite (FRC) sebagai bahan penyusun alat-alat tertentu seperti gigi tiruan cekat, restorasi onlay, splinting gigi goyah, pasak gigi dan space maintainer. Penyusun FRC terdiri dari fiber dengan jenis terbanyak glass fiber dan matriks berupa dental composite. Non dental glass fiber merupakan jenis glass fiber yang digunakan pada pembuatan gypsum, patung dan alat-alat otomotif yang mudah dijumpai di pasaran dengan harga terjangkau. Tujuan penelitian ini adalah untuk mengetahui potensi sitotoksisitas jenis dan lama perendaman non dental glass fiber reinforced composite terhadap sel fibroblas yang mati. Penelitian ini menggunakan FRC yang diperkuat oleh 3 jenis non dental glass fiber I, II, III dan dental E-glass fiber sebagai pembanding. Uji sitotoksisitas dilakukan dengan methyl tetrazolium test (MTT) menggunakan sel vero terhadap air hasil rendaman FRC selama 1, 4, 7 dan 10 hari masing-masing 6 pengulangan sampel tiap kelompok. Jumlah sel yang mati menunjukkan tingkat sitotoksisitas dan kemudian dianalisa dengan Anava dua jalur (α = 0,05).Hasil penelitian menunjukkan rata-rata kematian sel tertinggi yaitu 8,55 ± 0,27 % pada FRC III dengan lama perendaman 10 hari, sedangkan rata-rata kematian sel terendah yaitu 8,48 ± 0,35 % pada dental glass fiber dengan lama perendaman 1 hari. Berdasarkan pedoman dari Sjögren bahan tidak bersifat sitotoksis jika kematian sel masih dibawah 10%. Uji Anava dua jalur menunjukkan bahwa jenis non dental glass fiber reinforced composite dan lama perendaman mempunyai pengaruh tidak bermakna (p>0,05) terhadap sitotoksisitas sel fibroblas. Kesimpulan hasil penelitian yaitu non dental glass fiber reinforced composite tidak bersifat sitotoksis terhadap sel fibroblas, jenis non dental glass fiber reinforced composite dan lama perendaman tidak berpengaruh terhadap sitotoksisitas sel fibroblas
White Mineral Trioxide Aggregate (WMTA) using precipitated CaCO3 (PCC) from limestone has been synthesized. PCC in calcite structure was extracted from limestone by calcination at 900 °C for 3 h, dissolved in 0.8 M nitric acid solution and followed with carbonation for 60 minutes. PCC was used for the synthesis of WMTA by mixing with tetraethoxyorthosilicate, bismuth oxide, aluminum oxide, catalyst of with HNO3 and NH3 solution and thermally treated at 1100 °C for 3 h. The products were characterized with Thermal Gravimetric Analysis-Differential Thermal Analysis (TGA-DTG), X-ray Diffraction (XRD), Frontier-Transform Infrared (FTIR) spectroscopy, Scanning Electron Microscopy (SEM) and X-ray Fluorescence (XRF). The results showed that the PCC dominated calcite structure was obtained with 75.25% in yield and 99.42% in purity. The WMTA has been successfully synthesized by low thermal treatment at 1100 °C using catalysts of HNO3 and NH3 solution, proven by the presence of tricalcium silicate (C3S), dicalcium silicate (C2S), tricalcium aluminate (C3A), and Bi2O3 in WMTA.
Fiber reinforced composite is a material composed of matrix and reinforced by fiber. Fiber sisal is a natural fiber an alternatives synthetic fiber developed as dental material. Resin composite matrix is a hydrophilic substance that cause dimensional change. Alkalization of sisal fiber reduces the ability of hydrophilic sites which affects the dimensional changes. The aim of this study was to determine how different period of immersion affect dimensional change in samples. The samples used in this research were FRC made from flowable resin composite (Master Flow, Brazil), and alkalized sisal fiber. The samples were shaped into cuboid measuring 25x2x2 mm. Fiber was placed in the middle of sample with continuous unidirectional direction and then irradiated for 20 seconds using LCU. A total of 16 samples were divided to 4 groups, each group with the different period of immersion 0, 7, 14 and 21 days respectively. Dimensional changes were measured by the final dimension minus the initial dimension. Dimensional change was measured by the length, width, and height using digital sliding caliper with 0.001 mm nonius. The samples were immersed in the artificial saliva with pH 7. The data was analyzed using one way Anova and followed by LSD0.05. The result shows the mean value and standard deviation of dimensional changes with period of immersion at 0, 7, 14 and 21 days were 0.264±0.085, 2.856±0.089, 4.417±0.115 and 4.294±0.087 mm3. The F value obtained from one way Anova was 1.640±103 and the significance was 0.001 (p<0.05), indicated a significance difference. LSD presented a significance difference of mean to all treat,ent except for 14th and 21th day. This study concluded that various period of immersion increase effect to the dimensional changes of FRC with alkalized fiber sisal.
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