The nanoscale pop-in phenomena in polycrystalline α-Al 2 O 3 and single crystal α-Al 2 O 3 (0001) were comparatively investigated by nanoindentation with Berkovich indenters. It was found that different radii and loading rates have significant effects on the pop-ins formation, stress distributions and dislocation nucleations. Using the Hertzian contact theory and energetic model approach, the pop-in observations and resolved shear stress analysis are consistent with the explanation that the first pop-in corresponds to the nucleation of homogeneous dislocations when the theoretical shear strength is exceeded.

The fracture type differentiation, quantification, and source identification are desirable and yet intractable in the acoustic emission (AE) testing of a complex coating system. In this letter, a technique combining wavelet transform and conventional AE parameter analysis was developed to study the tensile failure process of thermal barrier coatings in real time. It is demonstrated that the failure of thermal barrier coatings originates from surface vertical cracking and follows interface cracking, and that the AE count increases with tensile load following a power law. The cracking source identified from AE signals agrees well with that observed by optical microscopy. This technique provides a powerful tool for the study of failure processes of a wide range of coatings and thin films.

The nanoscale elastic-plastic characteristics of the C plane of sapphire single crystal were studied by ultra-low nanoindentation loads with a Berkovich indenter within the indentation depth less than 60 nm. The smaller the loading rate is, the greater the corresponding critical pop-in loads and the width of pop-in extension become. It is shown that hardness obviously exhibits the indentation size effect (ISE), which is 46.7 ± 15 GPa at the ISE region and is equal to 27.5 ± 2 GPa at the non-ISE region. The indentation modulus of the C plane decreases with increasing the indentation depth and equals 420.6 ± 20 GPa at the steady-state when the indentation depth exceeds 60 nm. Based on the Schmidt law, Hertzian contact theory and crystallography, the possibilities of activation of primary slip systems indented on the C surface and the distributions of critical resolved shear stresses on the slip plane were analyzed.