New LA–ICP–MS zircon U–Pb geochronology, whole‐rock major and trace element geochemistry data, and petrographic observations are presented for three granitic dykes in the Changlingzi area of NE China. These data provide precise age and petrogenesis information with respect to the late Palaeozoic–Mesozoic intrusions in the area, which further constrain the geodynamic evolution of the southern Great Xing'an Range. Our zircon U–Pb data denote that the felsic dykes were emplaced during the Late Permian (~254 Ma) and Late Jurassic (143–142 Ma). Geochemically, the Late Permian monzonite porphyries are characterized by high Al2O3 (16.52–16.92 wt%) and Sr (490–579 ppm) contents and low Yb (0.52–0.57 ppm), Y (5.7–6.3 ppm), and heavy rare earth element (HREE) contents, which indicate an adakitic affinity. The Late Jurassic felsic dykes are characterized by high FeOt/MgO (8.2–11.9) and Ga/Al (3.3–3.8) ratios, high zircon saturation temperatures (888–929°C), and remarkable negative Eu (Eu/Eu* = 0.25–0.42) anomalies, indicating they are akin to A‐type granites. The Late Permian adakitic magma resulted from the partial melting of thickened lower crust, and was formed during collisional orogenesis related to subduction of Palaeo‐Asian Ocean crust. The Late Jurassic A‐type magmas were probably generated by the partial melting of amphibolite‐facies lower crustal materials. The melting occurred in response to the upwelling of asthenospheric material caused by collapse of thickened crust, due to gravitational instability during closure of the Mongol–Okhotsk Ocean. Subsequently, the latest stage of magmatic activity in this area and elsewhere in NE China was controlled mainly by subduction of Palaeo‐Pacific Ocean crust.
Nearly pure N2 fluid inclusions (Th (L) = −151~−168 °C; Th (V) = ~150.3 °C) were identified in W-mineralized quartz veins from the Yangjingou scheelite deposit, in the eastern Yanbian area, NE China. Other fluid inclusion populations include N2-CO2, NaCl-H2O ± N2 and CO2 ± N2-NaCl-H2O, but no hydrocarbons were detected. The host rocks are part of the Wudaogou Group metamorphic series, which mainly consist of Ca-rich mica schist. Subhedral sulfide minerals occur in early disseminated W-mineralized quartz veins, or have partially replaced early scheelite. ThN2 and ThN2-H2O indicate N2 fluid-trapping from 315 °C to 410 °C and from 80 MPa to 350 MPa. Oxygen and hydrogen isotopic data (δD = −74.9‰~−77‰, δ18O = 9.6‰~12‰, V-SMOW) suggest that the mineralizing fluids were composed of mixed magmatic and metamorphic water, N2-rich inclusions (δ15N = −0.5‰ to 1.4‰) indicate fluid-rock interaction with metamorphic rocks. The N2-rich fluid was closely associated with scheelite precipitation. During thermal decomposition under high oxygen fugacity conditions, which occurred synchronously with metamorphism and magmatic activity, large amounts of N2 were liberated from NH4+-micas, which then accumulated in the parent fluid of the quartz scheelite veins.
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