Alkaloids, saponins, steroid, terpenoid, flavonoids, phenolic distribution in 14 Malaysian favourite ulam and fruit belonging to different families were assessed and compared. The plants investigated wereparkia speciosa(petai),solanum torvum(terung pipit),pithecellobium bubalinum(kerdas),moringa oleifera(kacang kelor),dryobalanops oblongifolia(keladan),cosmos caudatus(ulam raja),mentha arvensis(pudina),ocimumsp. (selasih),cymbopogon nardus(serai wangi),eugenia polyantha(serai kayu),Barringtonia scortechinii, (Putat),musasp. (pisang),talinum paniculatum(akar som) andphyllanthus acidus(cermai).Moringa oleiferaleaf anddryobalanops oblongifoliafruit were found contain positive reactions of alkaloids. All the samples studied also show high content of saponin except in bark and seed ofparkia speciosaand stem ofphyllanthus acidus. Meanwhile, results of the phytochemical screening on saponins, steroids, terpenoids, phenolic and flavonoids showed thatcosmos caudatus,ocimum sp., mentha arvensis, barringtonia scortechiniiandmoringa oleiferawere the active compounds present in the leaves of the plant.