C-type asteroids1 are considered to be primitive small Solar System bodies enriched in water and organics, providing clues to the origin and evolution of the Solar System and the building blocks of life. C-type asteroid 162173 Ryugu has been characterized by remote sensing2–7 and on-asteroid measurements8,9 with Hayabusa2 (ref. 10). However, the ground truth provided by laboratory analysis of returned samples is invaluable to determine the fine properties of asteroids and other planetary bodies. We report preliminary results of analyses on returned samples from Ryugu of the particle size distribution, density and porosity, spectral properties and textural properties, and the results of a search for Ca–Al-rich inclusions (CAIs) and chondrules. The bulk sample mainly consists of rugged and smooth particles of millimetre to submillimetre size, confirming that the physical and chemical properties were not altered during the return from the asteroid. The power index of its size distribution is shallower than that of the surface boulder observed on Ryugu11, indicating differences in the returned Ryugu samples. The average of the estimated bulk densities of Ryugu sample particles is 1,282 ± 231 kg m−3, which is lower than that of meteorites12, suggesting a high microporosity down to the millimetre scale, extending centimetre-scale estimates from thermal measurements5,9. The extremely dark optical to near-infrared reflectance and spectral profile with weak absorptions at 2.7 and 3.4 μm imply a carbonaceous composition with indigenous aqueous alteration, matching the global average of Ryugu3,4 and confirming that the sample is representative of the asteroid. Together with the absence of submillimetre CAIs and chondrules, these features indicate that Ryugu is most similar to CI chondrites but has lower albedo, higher porosity and more fragile characteristics.

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The ExoMars rover, scheduled to be launched in 2020, will be equipped with a novel and diverse payload. It will also include a drill to collect subsurface samples (from 0‐ to 2‐m depth) and deliver them to the rover analytical laboratory, where it will be possible to perform combined science between instruments. For the first time, the exact same sample target areas will be investigated using complementary analytical methods—infrared spectrometry, Raman spectrometry, and laser desorption mass spectrometry—to establish mineralogical and organic chemistry composition. Fundamental for implementing this cooperative science strategy is the Raman Laser Spectrometer (RLS) calibration target (CT). The RLS CT features a polyethylene terephthalate disk used for RLS calibration and verification of the instrument during the mission. In addition, special patterns have been recorded on the RLS CT disk that the other instruments can detect and employ to determine their relative position. In this manner, the RLS CT ensures the spatial correlation between the three analytical laboratory instruments: MicrOmega, RLS, and MOMA. The RLS CT has been subjected to a series of tests to qualify it for space utilization and to characterize its behavior during the mission. The results from the joint work performed by the RLS and MicrOmega instrument teams confirm the feasibility of the “combined science” approach envisioned for ExoMars rover operations, whose science return is optimized when complementing the RLS and MicrOmega joint analysis with the autonomous RLS operation.

Near-infrared spectroscopy has become a well-known remote sensing technique for the surface characterization of planetary objects. Among them, Mars was observed in the past by three imaging spectrometers from orbit. The Infrared Spectrometer/SuperCam instrument performs near-infrared spectroscopy from the martian surface for the first time, with a 1.15 mrad field of view, in the 1.3 µm–2.6 µm range, enabling the identification of a variety of mafic and altered minerals. Before integration aboard the rover, the spectrometer underwent a calibration campaign. Here, we report the radiometric and linearity responses of the instrument, including the optical and thermal setups used to perform them over its nominal range of operations, in terms of instrument detector temperatures and spectral range. These responses were constrained by accuracy requirements (20% in absolute radiometry, 1% in relative). The derived instrument transfer function fits within these requirements (<15% in absolute and <0.8% in relative) and shall be used to calculate the expected instrumental signal-to-noise ratio for typical observation scenarios of mineral mixtures expected to be found in the Jezero crater, and ultimately to retrieve the spectral properties of the regions of interest observed by the rover.

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MicrOmega is a near-IR hyperspectral microscope designed to characterize in situ the texture and composition of the surface materials of the Hayabusa2 target asteroid. MicrOmega is implemented within the MASCOT lander (Ho et al. in Space Sci. Rev., 2016, this issue, doi:10.1007/s11214-016-0251-6). The spectral range (0.99-3.65 µm) and the spectral sampling (20 cm −1 ) of MicrOmega have been chosen to allow the identification of most potential constituent minerals, ices and organics, within each 25 µm pixel of the 3.2 × 3.2 mm 2 FOV. Such an unprecedented characterization will (1) enable the identification of most major and minor phases, including the potential organic phases, and ascribe their mineralogical context, as a critical set of clues to decipher the origin and evolution of this primitive body, and (2) provide the ground truth for the orbital measurements as well as a reference for the analyses later performed on returned samples.

Hayabusa2 spacecraft successfully collected rock samples from the surface of C-type near-Earth asteroid 162173 Ryugu through two touchdowns and brought them back to Earth in 2020. At the Extraterrestrial Sample Curation Center in JAXA, we performed initial description of all samples to obtain fundamental information and prepare the database for sample allocation. We propose morphological classifications for the returned samples based on the initial description of 205 grains described in the first 6 months. The returned samples can be distinguished by four morphological characteristics: dark, glossy, bright, and white. According to coordinated study to provide an initial description and detailed investigation by scanning electron microscopy and X-ray diffraction analysis in this study, these features reflect the differences in the degree of space weathering and mineral assemblages. The degree of space weathering of the four studied grain types is heterogeneous: weak for A0042 (dark group) and C0041 (white group); moderate for C0094 (glossy); and severe for A0017 (bright). The white phase, which is the mineral characteristic of the white group grains, is identified as large carbonate minerals. This is the first effort to classify Ryugu returned samples into distinct categories. Based on these results, researchers can estimate sample characteristics only from the information on the JAXA curation public database. It will be an important reference for sample selection for further investigation. Graphical Abstract