Antimony Sulphoiodide is most widely studied compound in group V-VI-VII family due to its large number of properties. Varoius methods of synthesis have been reported. We are the first to report synthesis of shiny SbSI crystals by the Chemical Vapor Deposition (CVD) technique using powder of Antimony, Sulphur and Iodine as the starting material. Needle shaped thin crystals of SbSI were found grown vertically on the walls of the quartz tube. Characterizations of the sample were done using different techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray analysis (EDAX). The charcteristcs peaks in
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