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ABSTRACT.A series containing ten (E)-4-(N-(4-cinnamoylphenyl)sulfamoyl)-3-(p-tolyl)-1,2,3-oxadiazol-3-ium-5-olates were prepared and examined their purities by literature method. The infrared and NMR spectral data were assigned and correlated with Hammett substituent constants and Swain-Lupton's constants using single and multi-regression analysis. From the results of statistical analyses the effects of substituents on the spectral data have been discussed.

ABSTRACT. About ten titled compounds were prepared by microwave assisted silica-phosphoric acid catalysed cyclization of substituted styryl 4-biphenyl ketones and urea under solvent-free conditions. The infrared frequencies (ν, cm -1 ) of NH 2 , C=N, COC stretches, NMR spectral chemical shifts(δ, ppm) of NH 2 , H 4-6 , C=N, and C 4-6 were assigned and correlated with Hammett substituent constants, F and R parameters using single and multi-regression analysis. From the results of statistical analysis, the effect of substituents on the infrared frequencies (ν, cm -1 ) and NMR chemical shifts (δ, ppm) has been studied.

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A series of 6-substituted quanoxaline derivatives have been synthesized and examined their purities by literature method. The infrared and 13 C NMR spectral data of these quinoxalines were correlated with Hammett substituent constants, F and R parameters using single and multi-regression analysis. From the results of statistical analysis, the effect of substituents on the spectral frequencies has been studied.