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A thorough experimental investigation of the effects of melt temperature and casting speed on the structure and defect formation during the steady and nonsteady stages of direct-chill (DC) casting of an Al-2.8 pct Cu alloy is performed. In addition, the temperature and melt-flow distributions in the sump of billets cast at different melt temperatures are numerically simulated and used in the discussion on the experimental results. Apart from already known phenomena such as the coarsening of the structure, deepening of the sump, and increased probability of bleed-outs during DC casting with increased casting temperature, a few new observations are made. The increased melt temperature is shown to increase the severity of subsurface segregation, whereas the macrosegregation in the rest of the billet remains virtually unaffected. Hot-tearing susceptibility is strongly diminished by an increased melt superheat. The amount and distribution of "floating" grains is demonstrated to depend on both the melt temperature and the casting speed. The porosity was found to only slightly depend on the melt temperature. The amount of nonequilibrium eutectic in the center of the billet increases with increasing melt temperature. The effects of melt temperature on the dimensions of the sump, transition region, and mushy zone and on the melt-flow pattern in the sump are discussed and used in the interpretation of experimentally observed phenomena.

Effects of casting speed and alloy composition on structure formation and hot tearing during direct-chill (DC) casting of 200-mm round billets from binary Al-Cu alloys are studied. It is experimentally shown that the grain structure, including the occurrence of coarse grains in the central part of the billet, is strongly affected by the casting speed and alloy composition, while the dendritic arm spacing is mostly dependent on the casting speed. The hot cracking pattern reveals the maximum hot-tearing susceptibility in the range of low-copper alloys (1 to 1.5 pct) and at high casting speeds (180 to 200 mm/min). The clear correlation between the amount of nonequilibrium eutectics (representing the reserve of liquid phase in the last stage of solidification) and hot tearing is demonstrated. A casting speed-copper concentration-hot-tearing susceptibility chart is constructed experimentally for real-scale DC casting. Computed dimensions of the solidification region in the billet are used to explain the experimentally observed structure patterns and hot cracking. Thermomechanical finite-element simulation of the solidifying billet was used as a tool for testing the applicability to DC casting of several hot-tearing criteria based on different principles. The results are compared to the experimentally observed hot tearing. It is noted that hot-tearing criteria that account for the dynamics of the process, e.g., strain rate, actual stress-strain situation, feeding rate, and melt flow, can be successfully used for the qualitative prediction of hot tearing.

Austenite nucleation and growth is studied during continuous heating using three-dimensional X-ray diffraction (3-D XRD) microscopy at the European Synchrotron Radiation Facility (ESRF) (Grenoble, France). Unique in-situ observations of austenite nucleation and growth kinetics were made for two commercial medium-carbon low-alloy steels (0.21 and 0.35 wt pct carbon with an initial microstructure of ferrite and pearlite). The measured austenite volume fraction as a function of temperature shows a two-step behavior for both steel grades: it starts with a rather fast pearlite-to-austenite transformation, which is followed by a more gradual ferrite-to-austenite transformation. The austenite nucleus density exhibits similar behavior, with a sharp increase during the first stage of the transformation and a more gradual increase in the nucleus density in the second stage for the 0.21 wt pct carbon alloy. For the 0.35 wt pct carbon alloy, no new nuclei form during the second stage. Three different types of growth of austenite grains in the ferrite/pearlite matrix were observed. The combination of detailed separate observations of both nucleation and growth provides unique quantitative information on the phase transformation kinetics during heating, i.e., austenite formation from ferrite and pearlite.

The microstructural evolution during continuous heating experiments has been studied for two C-Mn steels with carbon contents in the range 0.35 to 0.45 wt pct using optical microscopy, scanning electron microscopy (SEM), and electron probe microanalysis (EPMA). It is shown that the formation of the austenitic phase is possible in pearlite as well as in ferrite regions. Thus, a considerable overlap in time of ferrite-to-austenite and pearlite-to-austenite transformations is likely to occur. Another observation that was made during the experiments is that, depending on the heating rate, the pearlite-to-austenite transformation can proceed in either one or two steps. At low heating rates (0.05°C/s), ferrite and cementite plates transform simultaneously. At higher heating rates (20°C/s), it is a two-step process: first ferrite within pearlite grains transforms to austenite and then the dissolution of the cementite lamellae takes place. Several types of growth morphologies were observed during the experiments. The formation of a finger-type austenite morphology was noticed only for low and intermediate heating rates (0.05°C/s and 20°C/s), but not for the heating rate of 300°C/s. The formation of this fingertype austenite occurs on pearlite-ferrite grain boundaries and coincides with the direction of cementite plates. The carbon inhomogeneities in the microstructure affect the formation of martensitic/bainitic structures on cooling.