h i g h l i g h t s g r a p h i c a l a b s t r a c t Comprehensive 2D-LC was used to characterize polymeric nanoparticles.The relation between particle size and composition was determined.Applicable to hydrophobic, hydrophilic and charged monomercomprising particles. An algorithm was developed to automatically correct for HDC band broadening. Method can be used to study particle formation during emulsion polymerization.
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