The characteristics of gutta-percha (i.e., chemical compound and melting and glass transition temperatures) and the performance of laminated wood (i.e., moisture content, density, shear strength, and delamination ratio) prepared from sengon wood (Paraserianthes falcataria L. Nielsen) bonded with a gutta-percha-based adhesive were investigated. The gutta-perchabased adhesive was prepared by modification of gutta-percha with 5% maleic anhydride (MAH) and 0.75% benzoyl peroxide (BPO) at various gutta-percha to toluene ratios (w/w) (i.e., 15:85; 17.5:82.5; 20:80; and 22.5:77.5), followed by heating at 70 °C in a water bath for 10 min. Laminated wood was manufactured using both modified and unmodified gutta-percha-based adhesives at 250 gm -2 of glue spread and clamped for 24 h. Terpenes, especially 1,3 butadiene, 2-methyl (CAS)-isoprene (trans 1,4-isoprene) (polyterpene), were found to be the dominant chemical component of gutta-percha. The glass transition and melting temperatures of gutta-percha were -56.75 °C and 51.67 °C, respectively. The modification of gutta-percha with MAH and BPO as an initiator resulted in improved performance for the laminated wood. Infra-red spectrometry of the modified gutta-percha-based adhesive showed a new peak at 1720 cm -1 , indicating the C=O bond of MAH.
Activated carbon (AC) derived from coconut shells (CS-AC) was obtained through pyrolysis at 700℃ and subsequently activated with H3PO4. AC was ground in a Wiley mill several times to form powder particles at particle scales of 80, 100, and 200 meshes. The characterization of the AC was studied using scanning electron microscopy (SEM), X-ray diffraction analysis (XRD), Fourier-transform infrared spectroscopy (FT-IR), and surface area analysis (SBET). The CS-AC-200 mesh resulted in a higher percentage of mesopores and surface area. This particle size had a larger surface area with angular, irregular, and crushed shapes in the SEM view. The smaller particles had smoother surfaces, less wear, and increased curing depth and ratio of the hardness of the resin composite. Based on the characterization results of the AC, it is evident that CS-AC with a 200 mesh particle size has the potential to be used as a filler in biocomposites.
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