Column percolation tests may be suitable for prediction of chemical leaching from soil and soil materials. However, compared with batch leaching tests, they are time-consuming. It is therefore important to investigate ways to shorten the tests without affecting the quality of results. In this study, we evaluate the feasibility of decreasing testing time by increasing flow rate and decreasing equilibration time compared to the conditions specified in ISO/TS 21268-3, with equilibration periods of 48h and flow rate of 12mL/h. We tested three equilibration periods (0, 12-16, and 48h) and two flow rates (12 and 36mL/h) on four different soils and compared the inorganic constituent releases. For soils A and D, we observed similar values for all conditions except for the 0h-36mL/h case. For soil B, we observed no appreciable differences between the tested conditions, while for soil C there were no consistent trends probably due to the difference in ongoing oxidation reactions between soil samples. These results suggest that column percolation tests can be shortened from 20 to 30days to 7-9days by decreasing the equilibration time to 12-16h and increasing the flow rate to 36mL/h for inorganic substances.
Up-flow column percolation tests are used at laboratory scale to assess the leaching behavior of hazardous substance from contaminated soils in a specific condition as a function of time. Monitoring the quality of these test results inter or within laboratory is crucial, especially if used for Environment-related legal policy or for routine testing purposes. We tested three different sandy loam type soils (Soils I, II and III) to determine the reproducibility (variability inter laboratory) of test results and to evaluate the difference in the test results within laboratory. Up-flow column percolation tests were performed following the procedure described in the ISO/TS 21268–3. This procedure consists of percolating solution (calcium chloride 1 mM) from bottom to top at a flow rate of 12 mL/h through softly compacted soil contained in a column of 5 cm diameter and 30 ± 5 cm height. Eluate samples were collected at liquid-to-solid ratio of 0.1, 0.2, 0.5, 1, 2, 5 and 10 L/kg and analyzed for quantification of the target elements (Cu, As, Se, Cl, Ca, F, Mg, DOC and B in this research). For Soil I, 17 institutions in Japan joined this validation test. The up-flow column experiments were conducted in duplicate, after 48 h of equilibration time and at a flow rate of 12 mL/h. Column percolation test results from Soils II and III were used to evaluate the difference in test results from the experiments conducted in duplicate in a single laboratory, after 16 h of equilibration time and at a flow rate of 36 mL/h. Overall results showed good reproducibility (expressed in terms of the coefficient of variation, CV, calculated by dividing the standard deviation by the mean), as the CV was lower than 30% in more than 90% of the test results associated with Soil I. Moreover, low variability (expressed in terms of difference between the two test results divided by the mean) was observed in the test results related to Soils II and III, with a variability lower than 30% in more than 88% of the cases for Soil II and in more than 96% of the cases for Soil III. We also discussed the possible factors that affect the reproducibility and variability in the test results from the up-flow column percolation tests. The low variability inter and within laboratory obtained in this research indicates that the ISO/TS 21268–3 can be successfully upgraded to a fully validated ISO standard.
According to the mission scenario of the International Space Exploration Collaboration Group (ISECG), a "Mars sample return plan" is underway to bring the soil of Mars back to Earth by 2030. In the near future, in order to efficiently perform various operations on Mars (filling, excavation, sampling, ground improvement, etc.), presimulation on Earth will be important. Therefore, there is an urgent need to develop an appropriate simulated soil and to understand its material and mechanical properties. Based on this background, the authors are investigating the physical and basic mechanical properties of Mojave Mars Simulant soil (MMS-1), which has been reported as a simulated soil for Mars. This study focused on the particle shape of MMS-1 and was conducted to investigate the effect of particle shape on shear strength and volume change. As a result, it was revealed that MMS-1 has a higher shear strength than Toyoura sand and has a clear peak as the relative density increases. Moreover, MMS-1 is a material that causes volume expansion during shearing even for low stress and density states compared with artificial soil, and it was revealed that this is due to the angularity of the MMS-1 particles.
The disposal of 2011 Japan earthquake waste has become an important issue in Japan and it is not realistic or economical to send all of these wastes to landfill sites, due to limited space, high costs, and related environmental issues. In sustainable geotechnical applications, mixing of the separated soils from disaster wastes with additives (e.g., cement and fiber) is required to improve their strength and stiffness characteristics. In this study, monotonic triaxial drained compression tests are performed on medium dense specimens of Toyoura sand-cement-fiber mixtures with different percentages of fiber and cement (e.g., 0–3%) additives. The experimental results indicate that behavior of the mixtures is significantly affected by the concentration of fiber and cement additives. Based on a comprehensive set of test results, modifications to the series of equations were developed that can be used to evaluate the shear modulus and mobilized stress curves at small-strain levels. The experimental results and model comparison show that the elastic threshold strain (γe), reference strain (γr), increases with fiber and cement additives. In addition, the range of curvature parameter, from 0.88 to 1.0, provides a good comparison with the results of small-strain measurements. Overall, the comparison of the results and model shows that the small-strain measurements obtained using local strain transducers fall within the range of model upper and lower bound curves. The results of the unreinforced, fiber, and cemented sand shows a close agreement with the model mean curve, but fiber-reinforced cemented sand shows a good comparison with model upper bound.
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