In this study, a simple method to obtain pure β-phase directly from the melt process is proposed. A series of PVDF and ionic liquid (IL) was prepared by a solvent casting method with appropriate associated with the subsequent annealing treatment. IL plays a role of filler, which can create strong electrostatic interaction with PVDF matrix and directly induce β-phase crystallization on the PVDF during the melt. PVDF film sample is immersed in hot water for annealing treatment at different temperatures (25 °C to 70 °C). We found that annealing in high temperatures especially can not only increase more IL inserted into the amorphous region of polymer matrix to make more phase transformation, but also accelerate IL removal. Characteristics and performance of the PVDF films were investigated by use of FTIR, XRD, SEM, and AFM. Piezoelectric coefficient d33 as well as d31, degree of crystallinity, and sensitivity are measured in experiment to verify the performance of PVDF film.
Aluminum is a lightweight material that is commonly used in engine components. However, aluminum's low hardness and wear resistance, requires special treatment before being used as a component. Increasing the hardness and wear resistance of aluminum can be done by coating Titanium Nitride (TiN) with the sputtering method. In this study, the effect of sputtering time on Al-TiN coating on hardness and wear resistance was obtained. The deposition of titanium nitride thin films on aluminum using a gas ratio of Ar: N ((70:30%) with varied treatment times of 30, 60, 90, and 120 minutes. Hardness and wear resistance were observed using Vickers hardness tester and Ogoshi High-Speed Universal. Whereas the morphology of the wear surface was observed by SEM. The result shows that the treatment time of 60 minutes obtained the highest hardness and minimum specific wear rate.
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