Nanopore-based sensing has emerged as a promising candidate for affordable and powerful DNA sequencing technologies. Herein, we demonstrate that nanopores can be successfully fabricated in Mg alloys via focused electron beam (e-beam) technology. Employing in situ high-resolution transmission electron microscopy techniques, we obtained unambiguous evidence that layer-by-layer growth of atomic planes at the nanopore periphery occurs when the e-beam is spread out, leading to the shrinkage and eventual disappearance of nanopores. The proposed healing process was attributed to the e-beam-induced anisotropic diffusion of Mg atoms in the vicinity of nanopore edges. A plausible diffusion mechanism that describes the observed phenomena is discussed. Our results constitute the first experimental investigation of nanopores in Mg alloys. Direct evidence of the healing process has advanced our fundamental understanding of surface science, which is of great practical importance for many technological applications, including thin film deposition and surface nanopatterning.
In situ transmission electron microscopy was used to observe the dynamic evolution of the morphology and phase transformations in CuO nanowires during the process of sodiation. Our results facilitate a fundamental understanding of the sodiation mechanism in CuO nanostructures used as electrode materials in sodium ion batteries.
In this paper, using high resolution transmission electron microscopy, we showed the fabrication of faceted nanopores with various shapes in magnesium by focused electron beam (e-beam). The characteristics of nanopore shapes and the crystallographic planes corresponding to the edges of the nanopores were discussed in detail. Interestingly, by manipulating the e-beam (e.g., irradiation direction and duration), the nanopore shape and size could be effectively controlled along different directions. Our results provide important insight into the nanopore patterning in metallic materials and are of fundamental importance concerning the relevant applications, such as nanopore-based sensor, etc.
The atomic-scale oxide growth dynamics are directly revealed by in situ high resolution transmission electron microscopy during the oxidation of Mg surface. The oxidation process is characterized by the layer-by-layer growth of magnesium oxide (MgO) nanocrystal via the adatom process. Consistently, the nucleated MgO crystals exhibit faceted surface morphology as enclosed by {200} lattice planes. It is believed that the relatively lower surface energies of {200} lattice planes should play important roles, governing the growth mechanism. These results facilitate the understanding of the nanoscale oxide growth mechanism that will have an important impact on the development of magnesium or magnesium alloys with improved resistance to oxidation.
Abstract-This work presents extremely compact dual-mode and dual-band bandpass filter designs based on dual-resonance composite resonators developed by using integrated passive device (IPD) technology on a glass substrate.A dual-mode bandpass filter is also devised using a symmetric composite resonator with a perturbation element of grounding inductor to determine the filter bandwidth. Additionally, a feedback capacitive coupling path on the proposed dual-mode filter is implemented to produce three transmission-zero frequencies in the stopband. Furthermore, the proposed dual-band bandpass filter is designed in a high-density wiring transformer configuration with magnetic and electric mixed coupling. In addition to individually determining the fractional bandwidth of dual passbands, the magnetic and electric mixed coupling provides multiple transmission zeros to enhance the isolation between the two passbands and greatly improve the stopband rejection.
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