The largest antimonomolybdate
monomer, [Sb8MoVI
13MoV
5O66]5– (1-
Sb
8
Mo
18
), has been isolated and displays a new breakthrough of polyoxometalates
(POMs) with an ionothermal synthesis strategy. 1-Sb
8
Mo
18
features
the first hexanuclear sandwich-type polymolybdate (POMo) with an unexpected
metal ring {Sb6O12} to make its debut in Sb
clusters. Furthermore, 1-Sb
8
Mo
18
exhibits a prominent catalytic
activity for reducing nitrobenzene to aniline with excellent sustainability.
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