The inhibiting effect of N-furfuryl-N'-phenyl thiourea (FPTU) on the corrosion of mild steel in aqueous solutions of 0.05 and 0.1MHCl, as well as 0.025 and 0.05 M H2SO4 has been demonstrated using the potentiodynamic polarization technique. The polarization data showed that FPTU acts as an efficient anodic inhibitor for mild steel in both acid solutions. Avery high inhibition efficiency was evidenced in both acid solutions and it was found to vary with the concentration of the inhibitor and temperature. The obtained kinetic parameters of adsorption revealed spontaneous adsorption and a strong interaction of FPTU with the mild steel surface. .
Unidirectional carbon fiber-reinforced polymer nanocomposites were developed by adding alumina (Al2O3) and silicon carbide (SiC) nanoparticles using ultrasonication and magnetic stirring. The uniform nanoparticle dispersions were examined with a field-emission scanning electron microscope. The nano-phase matrix was then utilized to fabricate the hybrid carbon fiber-reinforced polymer nanocomposites by hand lay-up and compression molding. The weight fractions selected for Al2O3 and SiC nanoparticles were determined based on improvements in mechanical properties. Accordingly, the hybrid nanocomposites were fabricated at weight fractions of 1, 1.5, 1.75, and 2 wt.% for Al2O3. Likewise, the weight fractions selected for SiC were 1, 1.25, 1.5, and 2 wt.%. At 1.75 wt.% Al2O3 nanoparticle loading, the flexural strength modulus improved by 31.76% and 37.08%, respectively. Additionally, the interlaminar shear and impact strength enhanced by 40.95% and 47.51%, respectively. For SiC nanocomposites, improvements in flexural strength (12.79%) and flexural modulus (9.59%) were accomplished at 1.25 wt.% nanoparticle loading. Interlaminar shear strength was enhanced by 34.27%, and maximum impact strength was improved by 30.45%. Effective particle interactions with polymeric chains of epoxy, crack deflection, and crack arresting were the micromechanics accountable for enhancing the mechanical properties of nanocomposites.
The carbon fiber reinforced polymer composite has made a substantial impact on the manufacturing sectors owing to its excellent mechanical, thermal and corrosion resisting properties. The surface roughness mainly depends on the machining parameters while drilling of carbon fiber reinforced polymer composite laminates. The study concentrates on the impact of uncoated and titanium nitride coated solid carbide drills on minimizing the roughness that is generated while making holes in bi-directional carbon fiber reinforced polymer composite by optimizing the drilling constraints [spindle speed (A), feed rate (B), point angle (C) and drill diameter (D)]. Experimental studies are carried out using Taguchi L 27 orthogonal array. The investigation discloses that the drill diameter is one of the most influencing cutting parameters followed by spindle speed and feed rate. The response surface methodology is chosen as a tool for predicting and optimizing the process parameters. The investigation also discloses that the experimental and the predicted results of surface roughness are closely matching with each other. The surface morphology illustrates that titanium nitride coated solid carbide drills minimize the surface roughness compare to that of uncoated solid carbide drills.
The inhibition of corrosion of 304 SS in 2 N HCl solutions by N-furfuryl-N ' phenyl thiourea (FPTU) has been investigated using potentiodynamic polarization techniques. The results obtained reveal that FPTU performs excellently as anodic inhibitor (IE> 93%) for 304 SS in HCl solution. The inhibitor functions through adsorption following Temkin's adsorption isotherm, and the inhibition was governed by physisorption mechanism. The thermodynamic parameters deduced for the adsorption process reveal spontaneous adsorption of the compound on the alloy steel surface.
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