UPLC-MS and HPLC-VWD methods were used together for MC-LR determination in a wide concentration range. UPLC-MS can be applied in trace MC-LR determination, whereas HPLC-VWD is more suitable for high concentration range detection.
The g-C3N4QDs were synthesized by a simple solvothermal “tailoring” process from bulk g-C3N4 which have a “strong quenching” behaviour in the presence of TC. The proposed fluorescent sensor has been successfully applied to detect TC in actual samples.
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