International audienceThis papers aims to characterize the influence of moisture uptake on the mechanical behaviour of unidirectional flax fibre-reinforced epoxy laminates. Monotonic and cyclic tensile tests and free vibration characterization are carried out. Results show that LID flax-epoxy composites, when exposed to hygrothermal conditioning at 70 degrees C and 85% RH, exhibit a diffusion kinetic which follows a one dimensional Fickian behaviour. The mass uptake at equilibrium is approximately 3.3% and the diffusion coefficient 6.5 x 10(-6) m(2) s(-1). Water vapour sorption is shown to induce a significant change in the shape of the tensile stress-strain curve, a decrease in the dynamic elastic modulus of about 20% and a 50% increase in the damping ratio. Contrary to all expectations, water saturation does not degrade the monotonic tensile strength of such a flax-epoxy composites and leads to an increase in the fatigue strength for a high number of cycles. (C) 2016 Elsevier Ltd. All rights reserved
Achieving a complete curing of biocomposites without damaging fibers is very challenging. This study assesses the impact of processing upon the mechanical properties of a unidirectional flax reinforced epoxy composite and identifies which component (resin, reinforcement or interphase) is the most sensitive to post-curing at high temperature (100, 120 or 150°C). Post-curing temperature had a limited impact on the composite mechanical behavior excepted at 150°C where ultimate stress and strain decreased drastically while the stabilized modulus slightly increases. Post curing is responsible of a slight decrease of the matrix tensile properties attributed to the polymer oxidation but cannot explain on its own the evolution of the composite behavior. Interfacial adhesion played a minor role in the composite behavior probably due to its 2 intrinsic weakness. Finally, the flax fabric was highlighted to be the component most sensitive to thermal treatment thus governing the drop in the composite mechanical properties.
The development of composites based on vegetal fibers requires a good control of manufacturing process. The aim of this work is to determine the key parameters to produce high grade flax / epoxy unidirectional laminated composite by thermocompression. So, many processing parameters have been tested and ranked according to their influence on mechanical properties. Since variability can be high for this kind of materials, statistical analyses have been used to determine if properties variations were significant or not. Among all studied parameters, the three which have been identified as first rank influence on mechanical properties are: fibers conditioning, curing pressure and exit plate temperature.
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