Amino acid family crystals exhibit excellent nonlinear optical and electrooptical properties. L-Alanine single crystal belongs to the amino acid group and has been grown by the slow evaporation solution growth technique at room temperature. The grown crystals were characterized by high-resolution X-ray diffractometry (HRXRD), nuclear magnetic resonance (NMR), Fourier transform infrared (FTIR) spectroscopy, UV-Vis, Raman spectroscopy, mass spectra analyses and density measurements. Its laser damage threshold was measured and its nonlinear optical response was tested by using a Q-switched Nd:YAG laser, and the value of laser damage threshold is greater than that of potassium dihydrogen phosphate (KDP).
The potential organic NLO crystal of benzimidazole (BMZ) has been successfully grown by slow evaporation solution growth technique at room temperature. The crystalline perfection has been verified by High resolution X-ray diffraction (HRXRD) analysis. The very low angle boundary obtained for this solutiongrown specimen may be attributed to the segregation of solvent molecules (methanol), which were entrapped within the crystal during growth. The laser damage threshold has been measured by using high intensity Qswitched Nd:YAG laser. The observed value is greater than that of KDP and lesser than that of melt grown benzimidazole. The NLO efficiency has been determined and it is compared with the KDP crystal. The thermal behaviour has been assessed by TG/DTA analysis.
In this work, we report on the preparation of sodium dodecyl sulfate (SDS) surfactant added cobalt ferrite (CoFe 2 O 4 ) magnetic nanoparticles by a co-precipitation method at various concentrations (0.04, 0.08, 0.12, 0.16 and 0.20 M) of SDS. The formation of a single phase cubic spinel structure is confirmed by XRD analysis. FTIR study confirms the presence of Fe-O symmetrical stretching vibrations in the tetrahedral site. TEM images imply that the SDS surfactant significantly limits the agglomeration of CoFe 2 O 4 nanoparticles. A dielectric study reveals that the SDS added CoFe 2 O 4 has a higher dielectric constant than that of pure CoFe 2 O 4 nanoparticles. Magnetic measurements showed the enhanced saturation magnetization (138.75 emu g À1 ), coercivity (775.69 Oe) and retentivity (60.23 emu g À1 ) for 0.08 M SDS added CoFe 2 O 4 nanoparticles. Further, the results obtained in the present study suggest that the surfactant can significantly modify the size and morphology of the prepared CoFe 2 O 4 nanoparticles.
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