In this study, the Cr(VI) adsorption on modified polyaniline materials (MPM) was investigated. The MPM was produced by polymerization of aniline in 1 M H2SO4solution with the presence of activated tea residue. The tea residue samples have been activated by 0.5 KOH or H3PO4 (85 %) solution. The absorption of the Cr(VI) ions on the MPM was studied in this paperby means of infrared (IR) spectroscopy, scanning electron microscopy (SEM) and atomic adsorption spectrometer (AAS) in order to get a preliminary assessment of Cr(VI) adsorption efficiency. The experiment results shown that the applied MPM has good Cr(VI) adsorption capacity, the appropriate pH range for the adsorption process is 5.5÷7.5. The MPM after synthesis process is stable and easy to store and to apply for treatment of heavy metals in waste water.
Recently, plenty of interesting studies on improvement of bioavailability for poorly soluble drugs were implemented with different approaches such as using of combined biopolymers as a delivery system that allowed to enhancing drug solubility and bioavailability. In this work, alginate and chitosan were blended together in the form of polymeric particles, loaded with both lovastatin and ginsenoside Rb1 to producing the four-component nanoparticles by ionic gelation method. CaCl2 and sodium tripolyphosphate were used as gelation agent and cross-linking agent, respectively. The characteristics of obtained nanoparticles were studied by means of infrared spectra (IR), scanning electron microscopy (SEM), differential scanning calorimetry (DSC), and dynamic light scattering (DLS). In combination, ginsenoside Rb1 and lovastatin both interacted with each other to improve the drug release ability of the polymer particles. The change of initial content of drugs in the nanoparticles has a negligible effect on the functional groups in the structure of the nanoparticles but has a significant impact on drug release process of both lovastatin and ginsenoside Rb1 from the nanoparticles in selective simulated body fluids. In addition, the synergistic interaction of lovastatin and ginsenoside Rb1 could be also observed through the modification of relative crystal degree and drug release efficiency.
As the growing interest on green corrosion inhibitors, plant extracts have gradually showed the potential in replacing the traditional hazardous chemicals due to the eco-friendly and economy characteristics. Previous study reported that rose myrtle leaf-extract (Rhodomyrtus tomentosa, Myrtaceae) was as an efficient corrosion inhibitor for rust removal process of mild steel in H2SO4 acid medium. This study presents the corrosion inhibition assessments of rose myrtle leaf-extract on mild steel surface in HCl 1M solution. The potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) methods have been used to study the corrosion behaviors of mild steel. The corrosion rate, corrosion current and corrosion potential results indicate that only small amount of the leaf-extract (2% vol.) was required for high inhibition efficiency (Hin=83.9%). By affecting on both anodic and cathodic branches of the Tafel plot, the corrosion inhibition mechanism is proposed by an adsorption forming different barriers on the steel surface.Green inhibitor, Rhodomyrtus tomentosa, steel corrosion, EIS
In this study, Al-Mg alloy coatings were deposited on a C45 steel substrate by using the electric arc spray technique. The corrosion behavior of the coating was studied by electrochemical measurements and salt spray tests. The electrochemical tests were performed in 3.5 wt.% NaCl solution. Polarization tests indicated that the corrosion potential of the coating is significantly more negative than that of steel substrate after 240 hours of immersion. EIS measurements showed that after 24 hours of immersion, the total impedance increased with increasing the immersion time. This could be due to sealing of pores by corrosion products which hinder further penetration of the solution through the coating. Red rust spots did not appear on the surface of the coating after 1360 hours of salt spray test. The corrosion rate of the coating decreased with the increase in salt spray test time. After the salt spray test, the coating surface pitted and the cross section of the coating appeared with many long voids. In addition, XRD analysis proved that the main corrosion product was Al(OH)3. The results obtained indicated that arc thermal sprayed Al-Mg alloy coatings can reliably protect steel structures against corrosion in chloride-containing aqueous solutions.
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