A fine grain diamond film has been developed by microwave plasma assisted chemical vapor deposition. Various analytical techniques, including Rutherford backscattering, proton recoil analysis, Raman spectroscopy, and X-ray diffraction, were utilized to characterize the diamond films. The grain size of the film was determined from bright and dark field electron micrographs, and found to be 200–1000 Å. The films exhibited good optical transmission between 2.5 and 10 μm, with a calculated absorption coefficient of 490 cm−1. The friction coefficients of this film were found to be 0.035 and 0.030 at dry nitrogen and humid air environments, respectively, and the films had low wear rates.
The application of spectral and imagery diagnostics to YBa 2 Cu 3 O 7 (YBCO) laser-ablated plumes was systematically studied to determine their effectiveness for process control. Emission signatures were collected for plumes created by ablating bulk YBCO with a pulsed laser source. A KrF (λ=248 nm) laser source operating at 4-10 J/cm 2 at a 4-10 Hz pulse repetition frequency was used to ablate a bulk YBCO target at O 2 background pressures ranging from 50 to 400 mTorr. Emission spectra were collected over the 500 to 860 nm bandpass at distances from the target ranging from 31.4 to 55.0 mm. Of 87 observed emission lines, 76 were assigned to specific transitions with the aid of calibration lamps and reference to tables of energy levels. Line fluences were corrected for self-absorption, and electronic state distributions were calculated using the most recent NIST transition probabilities.
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