AISI 1018 mild steels are widely used for engineering applications in machine components and for structural purposes. These materials suffer mechanical damages especially when used under critical conditions of extreme load. In this study, the effect of austempering heat-treatment on the hardness, tensile strength, impact energy and the microstructure of AISI 1018 steels were evaluated. The steel specimens were subjected to austempering heat-treatment by austenitizing at a temperature of 830°C, maintained at this temperature for a period of 1 hour 30 minutes, before rapidly cooled down in a NaNO3 salt bath maintained at 300°C for isothermal transformation for a further 50 minutes before finally cooled down to room temperature. Microstructural analysis using Scanning Electron Microscope (SEM) shows transformation from ferrite/pearlite to bainite microstructure. The tensile strengths of the specimen increased from 400 MPa to 500 Mpa; hardness increased from an average value of 140Rc to 162Rc; while impact energy increased from 15.6 Joule to 30.6 Joule by the austempering heat-treatment. Keywords—Austempering, hardness, tensile strength, impact energy, microstructure
This article reports on the structure and electronic properties of carbon-rich polysilazane polymer-derived silicon carbonitride (C/SiCN) corresponding to pyrolysis temperatures between 1100 and 1600 °C in an argon atmosphere. Raman spectroscopy, X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDX), Scanning Electron Microscopy (SEM) and Hall measurements were used to support the structural and electronic properties characterization of the prepared C/SiCN nanocomposites. A structural analysis using Raman spectroscopy showed the evolution of sp2 hybridized carbon phase that resulted from the growth in the lateral crystallite size (La), average continuous graphene length including tortuosity (Leq) and inter-defects distance (LD) with an increase in pyrolysis temperature. The prepared C/SiCN monoliths showed a record high room temperature (RT) electrical conductivity of 9.6 S/cm for the sample prepared at 1600 °C. The electronic properties of the nanocomposites determined using Hall measurement revealed an anomalous change in the predominant charge carriers from n-type in the samples pyrolyzed at 1100 °C to predominantly p-type in the samples prepared at 1400 and 1600 °C. According to this outcome, tailor-made carbon-rich SiCN polymer-derived ceramics could be developed to produce n-type and p-type semiconductors for development of the next generation of electronic systems for applications in extreme temperature environments.
The concentration of inorganic chemical substances released into surface water from Okaba coal deposit were measured using spectroscopic techniques in order to assess the extent of pollution. Parameters measured (Pb, Fe, Cu, Cr, SO42-, Cl-, Mn, Zn and pH) showed that water samples within the mine area contain Pb, Fe, Cr, Cl-, Mn and Zn in concentrations beyond permissible intake limits; and the concentration of chloride measured (3000 mg/L) is capable of causing acid mine drainage (AMD). Concurrent evaluation of these inorganic substances using quantitative assessment reveal the possible presence of trace minerals like galena, sphalerite, chalcopyrite, pyrite and clay in Okaba coal deposit. Keywords— Acid mine drainage (AMD), Coal, Trace minerals, Water pollution
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