Abstract. Iron oxide has been the interest of many studies due to its applications in various scientific and industrial fields including in environment, corrosion, soil science, and exhaust emissions. Iron oxide (Fe2O3) has potential applications in catalytic reactions in electronic devices such as semiconductors, paint formulations, and lithium rechargeable batteries. Fe2O3 can be synthesized through the process of stirring, decomposition of organic iron, sol-gel, combustion, and evaporating solvents. Most of the methods used involve several steps and take a long time. The aim of this research was to investigate the phase and morphology characterization of iron oxide (Fe2O3) powder with solvent ethylene glycol after being sintered for 1 hour, 2 hours and 3 hours. The characterization tools utilized were XRD, SEM-EDX, and FTIR. The results of XRD analysis showed that the Fe2O3 sintered for 1 hour had the smallest crystallite size with a diameter of 21.05 nm. In the XRD test, the beam of X-ray was shot directly at the grain being tested. The results of SEM analysis showed thatthe Fe2O3 sintered for 1 hour produced the best result due to its crystallite size of 12.36 nm and hada shape of homogeneous nanosphere; the duration of sintering indeed had a great influence on the grain size of iron oxide (Fe2O3). In addition, the results of the elemental composition analysis indicate that the longer the sintering process, the higher the concentration of O but the lower the Fe.
This study aimed to enhance the properties of aluminiumsilicon (Al-Si) alloys by adding zinc oxide as a reinforcing material. This study was a type of pre-experimental design called the one-shot case study, in which sample groups subjects were given treatments and then observed. The steps included melting the aluminium-silicon in a furnace at 900° C, adding a certain amount of zinc oxide (0.05%, 0.1%, or 0.2%), stirring the mixture for 1 minute, and pouring it into a permanent mould. Results showed that, among the three specimens, the specimen reinforced with 0.2% zinc oxide had the highest tensile strength of 23.9 kg/mm 2 , the greatest hardness of 134.4 HV, and a flat surface with evenly distributed grains and more brittle fracture.
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