Abstract. Iron oxide has been the interest of many studies due to its applications in various scientific and industrial fields including in environment, corrosion, soil science, and exhaust emissions. Iron oxide (Fe2O3) has potential applications in catalytic reactions in electronic devices such as semiconductors, paint formulations, and lithium rechargeable batteries. Fe2O3 can be synthesized through the process of stirring, decomposition of organic iron, sol-gel, combustion, and evaporating solvents. Most of the methods used involve several steps and take a long time. The aim of this research was to investigate the phase and morphology characterization of iron oxide (Fe2O3) powder with solvent ethylene glycol after being sintered for 1 hour, 2 hours and 3 hours. The characterization tools utilized were XRD, SEM-EDX, and FTIR. The results of XRD analysis showed that the Fe2O3 sintered for 1 hour had the smallest crystallite size with a diameter of 21.05 nm. In the XRD test, the beam of X-ray was shot directly at the grain being tested. The results of SEM analysis showed thatthe Fe2O3 sintered for 1 hour produced the best result due to its crystallite size of 12.36 nm and hada shape of homogeneous nanosphere; the duration of sintering indeed had a great influence on the grain size of iron oxide (Fe2O3). In addition, the results of the elemental composition analysis indicate that the longer the sintering process, the higher the concentration of O but the lower the Fe.
Nanoreinforce materials such as ZnO, eggshell, Al2O3, TiO2, and ZrO2 have been shown to improve the mechanical properties of Al-Si alloy. Nanomaterial Fe2O3 has many applications as catalysts reaction in electronic devices, for example, semiconductor materials, paint formulations, lithium rechargeable batteries, and is often applied in industrial fields. It is known that Fe2O3 can be synthesized through the stirring process on machine and method used will involve several steps that relatively take a long time. In this study, Al-Si alloy reinforced by using nanomaterial Fe2O3 which sintered at a temperature of 600C for 3 hours aimed to improve mechanical and morphological properties of Al-Si alloy. The method used was stir casting, where this method was known as flexible, simple, and economic. The result of reinforcing Al-Si alloy by using nanomaterial Fe2O3 had affected on the hardness level of Al-Si alloys as evidenced by the fracture morphology that was brittle and had a light reflection.
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