According to the mechanism of thermal insulation, closed pore perlite, hollow glass microsphere and nanoantimony tin oxide (ATO) powder three different kinds of functional fillers were adopted respectively to prepare obstructive, reflective and radiative thermal insulation coating base on polyvinylidene fluoride emulsion, and how the category and content of functional fillers effect the thermal insulation performance of the fluorocarbon thermal insulation coating (FTIC) was investigate. The test results showed that, all the three functional fillers has an significant effect on the thermal insulation performance of FTIC.
TiO2 nanorod array films with or without Nb doping grown directly on transparent conductive glass (FTO) were prepared by a facile hydrothermal method. The films were characterized by means of field emission scanning electron microscopy (FE-SEM) with energy-dispersive x-ray spectra (EDS), X-ray diffraction (XRD) and the X-ray photoelectron spectroscoy (XPS). The electrochemical impedance spectroscopy (EIS), linear sweep voltammetry (LSV) and transient photocurrent were investigated in a three-electrode system with TiO2 nanorod array film served as the photoanode. The photoelectrocatalytic activity of the films was evaluated by the oxidation of glucose under UV irradiation. The results show that both the pure and Nb-doped TiO2 nanorods perpendicularly grown on FTO substrate are rutile phase. The resistance of the TiO2 nanorod array photoanode is decreased significantly by Nb doping. The steady-state photocurrent (iss) for glucose oxidation at Nb-doped TiO2 nanorod array film is much higher than that at the pure one. The enhanced photoelectrocatalytic activity of the Nb-doped TiO2 nanorods could be attributed to the enhanced charge transport ability.
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