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Sediment samples obtained from pits in the Mbiame floodplain gemstone prospect in the northwestern part of Cameroon were studied for their bulk geochemical properties together with the mineral composition of the gemstones found therein to decipher their provenance. Five main layers were isolated in each pit comprising an organic rich humus layer, muddy layer, unconsolidated and poorly sorted sandy layer, clay layer and gravel layer. The gravel layer is the most high-yielding in terms of gemstones content. The sediments have high rare earth element (REE) concentrations varying between 135 and 456 ppm with variable light/heavy rare earth element (LREE/HREE) ratio values (5.8-21.5). REE chondrite normalized patterns show similar high LREE enrichment and no Eu anomalies (Eu/Eu* = 0.9 − ~ 1) for all samples. The gemstones selected from the various horizons range in color from light gray, light blue/green, dark blue, pale brown and red. Some of the grains have zircon and ilmenite mineral inclusions while some of the zoned grains show simple core-rim zonation as well as oscillatory and sectorial zoning patterns. Bulk sediment geochemistry of sediments from the Mbiame gem prospect suggests an igneous provenance generally of felsic intermediate source input. The alluvial gemstones from the Mbiame gem prospect are the sapphire variety of corundum and the grains combined with zircon and ilmenite inclusions and megacrysts suggest a derivation from felsic to intermediate igneous rocks.

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