Power characteristics for an agitated vessel equipped with planar short baffles of length L and pitched blade turbine of pitch β are presented in the paper. The studies were carried out in the vessel of inner diameter D = 0.6 m, where the baffles were located in the distance p from the vessel bottom (p + L = H). Torque was measured using strain gauge method within the turbulent regime of the flow of Newtonian liquid in the agitated vessel. The effects of the pitch β and geometrical parameter p/H on the power number Ne were determined mathematically. The results showed that, for the assumed value of the angle β, the function Ne = f (L/H) decreases with the decrease in the baffle length L (i.e. with the increase in the parameter p). Moreover, for the assumed value of the baffle length L, the function Ne = f (β) increases with the increase in the angle β of the inclination of the impeller blade.

The results of the power consumption for an agitated vessel equipped with vertical tubular baffles and high-speed impeller are presented in the paper. Aqueous solutions of CMC were agitated within transitional range of the non-Newtonian liquid flow in the agitated vessel of inner diameter equal to 0.6 m. Eight different types of the impellers were tested: Rushton or Smith turbines, turbine with straight blades, pitched blade turbines and propeller. The J tubular baffles of outer diameter B were located in the position e from the vessel wall. Different configurations of baffles, arranged around the vessel circumference singularly or blocked in the modules, were considered in the study. In total, 180 different tubular baffles–impeller systems were tested. The measurements of the torque were conducted by means of the strain gauges method. Based on the power characteristics obtained for each impeller type, the effect of the geometrical parameters of the vertical tubular baffles on the power number was determined and discussed. The results show that geometry of the tubular baffles mostly affects the power number for the system with radial flow Rushton turbine. Moreover, power numbers decrease with the increase of the clearance between baffle and vessel wall for the systems, in which the radially axial circulation of the liquid is promoted. The dependences of the power number on the geometrical parameters of the vertical tubular baffles arranged singularly around the vessel circumference were described by means of the Eqs. (5)–(16). These equations can be useful in the project computations.

Results of the experimental research on gas hold-up, power consumption for liquid phase and gas—liquid systems, and on residence time of the gas bubbles are presented in the paper for an agitated vessel with a turbine impeller. Distilled water or aqueous solutions of NaCl were used as the liquid phase. Air was dispersed into liquid as the gas phase. The studies were carried out in an agitated vessel of the inner diameter D = 0.634 m. Tubular baffles of the diameter of 0.7D, consisting of 24 vertical tubes of the diameter of 0.016D, were located inside a flat-bottomed tank. Turbines with six blades and the pitch of 90°, 60°, or 45°, respectively, were used for agitation. Measurements were carried out in the range of good dispersion of gas bubbles in the liquid within the turbulent regime of the liquid flow. Effects of the gas bubbles capability to coalesce on the gas hold-up, residence time of the gas bubbles, and power consumption were analyzed. Results of the power consumption (P G-L/P o = f 1(Kg, Fr)) and gas hold-up (φ= f 2(Kg, We, Y)) were approximated mathematically, using Eqs. (5) and (6), respectively. In Eq. (6), parameter Y was introduced in order to describe the influence of the bubbles capability to coalesce on the gas hold-up. The results of the study show that power consumption does not depend on the capability of bubbles to coalesce, but the pitch of the turbine impeller affects the power characteristics in such a physical system significantly. However, the residence time of the gas phase in agitated liquid depends on the pitch of the impeller blade and on the capability of bubbles to coalesce.

No abstract

A comparative analysis concerning the influence of different factors on momentum transfer in mechanically agitated systems was carried out on the basis of experimental results for solid-liquid, gas-liquid and gas-solid-liquid systems. The effects of the impeller -baffles system geometry, scale of the agitated vessel, type and number of impellers and their off-bottom clearance, as well as physical properties of the multiphase systems on the critical impeller speeds needed to produce suspension or dispersion, power consumption and gas hold-up were analysed and evaluated.

Experimental results of gas hold-up, power consumption and residence time of gas bubbles in a gas-solid-liquid system produced in an agitated vessel equipped with a high-speed impeller and a vertical tubular coil are presented in this paper. Critical agitator speed, needed for the dispersion of gas bubbles and solid particles in liquid were also identified. The studies were carried out in an agitated vessel of the inner diameter D = 0.634 m and the working liquid volume of about 0.2 m3. A tubular coil of the diameter of 0.7D, consisting of 24 vertical tubes of the diameter of 0.016D, was located inside the flat-bottomed vessel. The agitated vessel was equipped with a Rushton turbine with six blades or an A 315 impeller with four blades. Both impellers had diameter, d, equal to 0.33D. The vessel was filled with liquid up to the height H = D. In this study, air and particles of sea sand with the mean diameter of 335 μm and the concentration of up to 3.0 mass % were dispersed in distilled water as the liquid phase. The measurements were carried out within the turbulent regime of the fluid flow in the agitated vessel. Results of the measurements were processed graphically and mathematically. Lower values of the critical agitator speed, n JSG, needed for simultaneous dispersion of gas bubbles and particles with the solids concentration from 0.5 mass % to 2 mass %, were obtained for the vessel equipped with the A 315 impeller. Higher values of the specific power consumption were reached for the vessel with the Rushton turbine. Higher values of the gas hold-up and residence time of the gas bubbles in the fluid were obtained for the system equipped with the Rushton turbine. Results of the gas hold-up as a function of the specific power consumption, superficial gas velocity and solids concentration were approximated with good accuracy using Eq. (5).

Results of drops dimension and rheological properties of the produced multiple emulsion are presented in this paper. Sunflower oil (oil phase), distilled water (liquid phase), and lecithin from soya beans were used as materials to produce emulsion. Emulsions were produced in vessel with inner diameter D = 0.1 m and liquid height H = 0.5D. Smith turbine has been used to stir the emulsions. Examination of the drops dimension and rheological properties were conducted for emulsions collected after 15 min and 45 min of stirring as well as after the 3rd and 30th day. There were 6 measurements altogether. To do the analysis of drops dimension, in each series 700-800 inner oil-phase drops were taken. The results were presented in a form of graphics as a distribution of drops. The dimensions of the drops obtained d were also presented as a minimal diameter d min , arithmetic mean diameter d a , median d m , and Sauter mean diameter d 32. The results of the research of rheological emulsions were presented graphically as a viscosity curve and they were described by Herschel-Bulkley model (Eq. 4) Keywords Multiple emulsion • Microscopic analysis • Rheological measurements List of symbols B Width of the baffles (m) D Inner diameter of the vessel (m) d s Diameter of the stirrer (m) d Diameter of the drop (µm) d a Arithmetic mean diameter of the drop (µm) d m Mediana diameter of the drop (µm) d 32 SAUTER mean diameter (µm) d 43 Volume-weighted mean diameter (µm) H Liquid height in the vessel (m) J Number of baffles n Stirrer speed Z Number of stirrer blades (s −1) Greek letters τ Shear stress (Pa) γ Shear rate (s −1)

The aim of the study presented was to experimentally analyze an effect of the nutrient type and its concentration on the variability of rheological properties of the baker's yeast suspensions for different time periods. Aqueous suspensions of the baker's yeast of various concentration (solution I, without nutrient) and yeasts suspended in aqueous solution of sucrose or honey as nutrients with different concentration (solution II or solution III) were tested. Experiments were carried out using rotational rheoviscometer of type RT10 by a company HAAKE. The measurements were conducted for different time periods (from 1 h up to 144 h) at given fl uid temperature. On the basis of the obtained data, rheological characteristics of the aqueous solution of baker's yeast suspensions without and with nutrients of different sucrose or honey concentration were identifi ed and mathematically described.