In this research work, copper and CNTs have been processed using high energy milling in different milling times (5, 10 and 15 hours). FESEM and XRD have been used to characterize the milled powders. The FESEM micrographs of the milled powders indicated that the morphology of powders changed from spherical shape to flake as milling time increased. The effect of sintering temperature as well as CNTs content on the properties of Cu-CNTs nanocomposite has been investigated. The optimum sintering temperature to produce Cu-CNTs nanocomposites is determined to be 900 o C. The microstructure and phase analysis of Cu-CNTs nanocomposites were studied by field emission scanning electron microscopy and X-ray diffraction. Mechanical properties of nanocomposite samples at various sintering temperatures were investigated. Cu-CNTs nanocomposite with 4 vol.% CNTs fabricated by powder metallurgy method indicated the highest value of the microhardness and bending strength as compared to pure copper.
In this research, multiwall carbon nanotubes were dispersed in a copper matrix using a planetary ball mill. The mixed powders were compacted using a uniaxial hydraulic presser. A novel method of microwave sintering was applied to consolidate Cu-CNT nanocomposites Conventional sintering method was also used to sinter samples to investigate the effects of applied methods on the properties of the sample. Sintering time was reduced to 20 min using microwave sintering method. The morphology and phase analysis of nanocomposites were studied by FESEM and XRD. The physical and mechanical properties of Cu-CNT nanocomposites were characterized using electrical conductivity, bending strength, and micro-hardness. The results show that the mechanical properties of Cu-CNT nanocomposites are improved significantly by microwave route. The optimum hardness and bending strength were obtained for 4 vol. % CNT as an optimum amount of reinforcement.
In this research, copper (Cu)-carbon nanotubes (CNTs) nanocomposites were synthesized with different weight percentages of CNTs by double pressing double sintering (DPDS) method as well as conventional sintering method. A planetary ball mill was used to disperse CNTs in Cu matrix. The milled powders were first cold pressed to 450 MPa in a uniaxial stainless-steel die with cylindrical compacts (diameter: 12 mm and height: 5 mm). The effect of CNTs content and the DPDS method on the properties of the nanocomposites were investigated. The microstructure and phase analysis of Cu-CNTs nanocomposite samples were studied by FESEM and X-Ray Diffraction. The electrical conductivity of nanocomposites was measured and compared to both sintering methods. Mechanical properties of Cu-CNTs nanocomposites were characterized using bending strength and micro-hardness measurements. Enhancements of about 32% in bending strength, 31.6% in hardness and 19.5% in electrical conductivity of Cu-1 wt.% CNTs nanocomposite synthesized by DPDS method were observed as compared to Cu-1 wt.% CNTs nanocomposites fabricated under the similar condition by a conventional sintering process.
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