Trifluoroacetic anhydride – sodium iodide mixture (TFAA-I) reacts with nitrones with the release of iodine. Since stoichiometrical amounts of iodine are formed with respect to starting nitrones, TFAA-I reagent can be used for analytical determination of nitrones. Two procedures for the determination of nitrones (on μ mole and on nmole scale) have been described. Keywords: nitrones determination, TFAA-I reagent.
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