The influence of regime (temperature, composition of gas mixture and its pressure) and energy characteristics (voltage, current density, specific discharge power) at hydrogen-free-nitriding in a glow discharge (HFNGD) on the structure, phase composition of nitrided layers is investigated. It is shown that due to the combination of regime and energy parameters of HFNGD it is possible to achieve physical and chemical indicators of nitrided layers set by operating conditions. The set of traditionally fixed values of regime parameters (temperature, gas mixture connection, pressure and saturation time) without taking into account energy characteristics (voltage, current density and specific discharge power) significantly reduces the technological capabilities of HFNGD. With controlled regulation of the energy characteristics of HFNGD, a significant reduction in the energy consumption of the nitriding process is achieved. It is established that the energy levels of the main subprocesses differ significantly: the formation of nitrides occurs at low energies, surface sputtering is realized at high voltage values, and nitrogen diffusion occurs at high current densities. In cases where the flow energy is insufficient, either a glow discharge may not occur at all, or at insufficient stress the nitride layer on the surface is not sprayed and it acts as a barrier that prevents the diffusion process into the inner layers of the metal, leading to low physicochemical indicators of nitrided layers. The priority in the formation of one or another phase (, , u, ), the quantitative ratio between them and the required performance properties of the metal, respectively, can be achieved only through an independent combination of energy and regime characteristics of HFNGD.
PurposeThe purpose of this article is the development of up-to-date equipment for making nanocomposites for investigation of the antimicrobial properties of nanotextiles and the creation of a scientific base to choose materials of clothing with a special purpose.Design/methodology/approachInvestigations are focussed on modifying the surface of textile materials by metal ions nanoparticles (AgJ, CuJ). The work of the equipment is based on the creation of metal nanocomposites in polyethyleneglycol (PEG). It is heated up to a temperature of not more than 130ºС, followed by adding the dispersion of metal in small portions to water. Nanoparticles are uniformly distributed on material surface that provides the improvement of its characteristics.FindingsIt has been found that modifying natural fibrous materials by nanoparticles of metal ions (AgJ, CuJ) promotes increasing their bactericidal and fungicidal properties with a comparison with traditional cotton materials. Microbiological investigations of antimicrobial properties of the cotton fabric have been conducted according to their effects on staphylococcus bacteria, E. coli and fungi.Research limitations/implicationsThis research is limited to cotton fabrics. Therefore, other fabric types can be investigated to expand the data basis in the future.Practical implicationsThe main practical point of developed equipment is that it can be used for obtaining bactericidal and fungicidal properties of natural and fibrous materials modified by nanoparticles of metal ions (AgJ, CuJ). That provides new characteristics of textile materials that can be used in the future for special clothing tailoring.Social implicationsThe use of engineering equipment will allow in perspective to produce clothes with bactericidal and fungicidal properties, which can improve people’s lives through the prism of health and finished product quality.Originality/valueSpecial equipment for investigation of antimicrobial properties of nanomodified textile materials of different kinds has been engineered, and there is an opportunity to create materials with antibacterial and antifungal properties. The application of this equipment provides the receiving of new characteristics for textile materials with silver ions nanoparticles. Such properties of nanomodified materials are useful for human health and can be used in the production of various textile products.
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