The objective of this study was to determine the degree of conversion (DC), hardness (H), and modulus of elasticity (E) of a dual-cured resin cement, a light-cured resin cement, and a flowable resin cured through opaque or translucent ceramic with different exposure times. RelyX ARC (dual), RelyX Veneer (light-cured), and Filtek Z350 Flow resin specimens 0.5 mm thick were cured for 40, 80, and 120 seconds through 1-mm thick translucent or opaque feldspathic ceramic disks (n=10). The specimens were stored at 37°C for 24 hours. Half of each specimen was used to test the DC and the other half to test H and E. The DC was determined in a Fourier transform infrared spectrometer in absorbance mode at peaks of 1638 cm(-1) and 1610 cm(-1). H and E were determined using nanoindentation with one loading cycle and a maximum load of 400 mN. The data were analyzed with three-way analysis of variance (ANOVA), the Games-Howell test, and the Pearson correlation test (α=0.05). Statistically significant differences were found for all three factors (material, opacity, and exposure time), as well as interaction between them. The opaque ceramic resulted in lower DC, H, and E than the translucent ceramic for an exposure time of 40 seconds. An exposure time of 120 seconds resulted in a similar DC for all materials, irrespective of the opacity of the ceramic. Materials cured for 120 seconds had higher H and E than those cured for 40 seconds. The exposure time and opacity of the ceramic exerted an influence on the DC, H, and E of the materials evaluated.
Aim
The objective of this study was to evaluate the effect of light polymerization on water sorption and solubility of hybrid composites.
Methods and Materials
Three composite resins were used to make discs cured with either quartz-tungsten halogen (QTH) or light emitting diode (LED) curing units. The specimens were stored in a desiccator at 37°C and weighted to a constant mass, then immersed in deionized water for different periods of time, and reconditioned until achieving a constant mass. Sorption and solubility were calculated and subjected to analysis of variance (ANOVA) and Tukey tests (p<0.01).
Results
There were no statistically significant differences between the light sources. Water sorption increased with storage time for all the composites. The lowest sorption was observed for Herculite XRV™, followed by Tetric Ceram™, and Filtek Z250™. Increased storage times reduced the solubility of Filtek Z250™ but did not affect the solubility of Herculite XRV™ and Tetric Ceram™.
Conclusion
Water sorption and solubility of composites are not affected by the type of polymerization when the same intensity and exposure times are used. Thus, the differences found are probably related to the composition of the materials.
Clinical Significance
Water sorption and solubility of composites can lead to a shortened service life. However, these properties are not correlated to the type of polymerization.
Citation
Archegas LRP, Caldas DBM, Rached RN, Vieira S, Souza EM. Sorption and Solubility of Composites Cured with Quartz-tungsten Halogen and Light Emitting Diode Light-curing Units. J Contemp Dent Pract 2008 February;(9)2:073-080.
The aim of this study was to detect and quantify the main residual monomers released from composites, using high performance liquid chromatography (HPLC). Discs were made with dental composites (Herculite XRV, Tetric Ceram and Filtek Z250)
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