The keyhole mode in laser powder bed fusion (LPBF) additive manufacturing can be associated with excessive porosity and spatter, however, the underlying physics in multilayer build conditions remain unclear.Here, we used ultra-fast synchrotron X-ray imaging to reveal this phenomena. We revealed melt pool dynamics, keyhole porosity and spatter formation mechanisms and their impact in all layers of the build. We observed that the transient melt pool dynamics associated with the keyhole include: (I) keyhole initiation, (II) keyhole development, and (III) melt pool recovery. Porosity and spatter were associated with stages (II) and (III). We also discovered that droplet spatter can form due to the collapse of the keyhole recoil zone, causing molten particle agglomeration and ejection during stage (III). Our results clarify the transient dynamics behind the keyhole mode in a multi-layer LBPF process and can be used to guide the reduction in porosity and spatter in additive manufacturing.

Porosity and high surface roughness can be detrimental to the mechanical performance of laser powder bed fusion (LPBF) additive manufactured components, potentially resulting in reduced component life. However, the link between powder layer thickness on pore formation and surface undulations in the LPBF parts remains unclear. In this paper, the influence of processing parameters on Ti-6Al-4V additive manufactured thin-wall components are investigated for multilayer builds, using a custom-built process replicator and in situ highspeed synchrotron X-ray imaging. In addition to the formation of initial keyhole pores, the results reveal three pore phenomena in multilayer builds resulting from keyhole melting: (i) healing of the previous layers pores via liquid filling during remelting; (ii) insufficient laser penetration depth to remelt and heal pores; and (iii) pores formed by keyholing which merge with existing pores, increasing the pore size. The results also show that the variation of powder layer thickness influences which pore formation mechanisms take place in multilayer builds.High-resolution X-ray computed tomography images reveal that clusters of pores form at the ends of tracks and when variations in the layer thickness and melt flow cause irregular 2 remelting and track height undulations. Extreme variations in height were found to lead to lack of fusion pores in the trough regions. It is hypothesised that the end of track pores were augmented by soluble gas which is partitioned into the melt pool and swept to track ends, supersaturating during end of track solidification and diffusing into pores increasing their size.

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Marangoni flow has a substantial influence on the quality of components fabricated via laser powder bed fusion (LPBF). However, Marangoni flow in melt pools is rarely quantified due to the opacity of liquid metals and the necessity for in situ evaluation. Here we report the findings of high-temporal-resolution synchrotron x-ray radiography experiments tracking the flow in the melt-pool. Dense, highly attenuating tungsten carbide particles are seeded within an elemental powder blend of aluminium and copper of varying composition. Due to the extremely high temporal resolution of greater than 50 kfps at the 31-ID-B beamline at the Advanced Photon Source, USA, we can track the position of tracer particles from frame to frame. This data provides valuable process guidance for optimising mixing and informs the development and validation of multiphysics models.

The Directed Energy Deposition Additive Manufacturing (DED-AM) of SS316L was studied using in situ and operando synchrotron X-ray imaging to quantitively understand the effect of processing parameters on the melt-pool morphology and surface quality. It was found that surface roughness of DED-AM builds can result from melt pool surface perturbations caused by changes in the melt flow and build stage motion perturbations. Process maps are developed that quantitatively correlate build quality to process parameters including powder feed rate, laser power and traverse speed. How the AM process parameters control build efficacy is clarified, and the processing conditions required to dampen surface perturbations leading to roughness were determined.

Directed Energy Deposition Additive Manufacturing (DED-AM) is one of the principal AM techniques being explored for both the repair of high value components in the aerospace industry as well as freeform fabrication of large metallic components. However, the lack of fundamental understanding of the underlying process-structure-property relationships hinders the utilisation of DED-AM for the production or repair of safety-critical components. This study uses in situ and operando synchrotron X-ray imaging to provide an improved fundamental understanding of laser-matter interactions and their influence on the melt pool geometry. Coupled with process modelling, these unique observations illustrate how process parameters can influence the DED-AM melt pool geometry. The calibrated simulation can be used for guidance in an industrial additive manufacturing process for microstructure and quality control.

With recent advances in manufacturing methods for metals with defined, complex shapes, the investigation of metallic lattice materials (metals containing significant porosity with a regular arrangement of the solid, frequently in the form of thin structural members or struts) has become more common. These materials show many interesting properties, and may have the capacity to be more highly engineered and optimized for a given application than the random structures of other microcellular metals, such as metallic foams and sponges, permit. However, the novel structure brings new structure-properties correlations to bear on the mechanical behavior of the materials. This paper examines one type of lattice, made from titanium alloy (Ti6Al4V) and fabricated by Electron Beam Melting (EBM), a material which typically shows only limited plasticity on deformation. The overall mechanical response is governed by the cooperative deformation of a very large number of individual struts that make up the lattice, and thus there is great potential for significant impact from damage arising due to defects in individual struts in the assembly. We explore the effect of simulated processing defects (missing struts) on the lattice properties, and how deformation and failure is distributed across the lattice after the onset of failure. To gain knowledge of how lattices deform, samples of various geometries, designed to probe compression, indentation-compression and tension (in the form of bending) are produced and tested under Digital Image Correlation (DIC) mapping. The understanding gained here will be of great use in designing new metallic lattice structures with greater damage tolerance and resistance to failure.