In this study, gelatin and pullulan were successfully prepared as a novel type of protein–polysaccharide composite nanofibrous membrane by electrospinning at room temperature with deionized water as the solvent. The effects of gelatin content on the properties of the solution, as well as the morphology of the resultant nanofibers, were investigated. Scanning electron microscopy (SEM) was utilized to observe the surface morphology. Fourier transform infrared spectroscopy (FTIR) was used to study the interaction between gelatin and pullulan. Incorporation of pullulan with gelatin will improve the spinnability of the mixed aqueous solution due to lower surface tension. Moreover, the conductivity of the solution had a greater effect on the fiber diameters, and the as-spun fibers became thinner as the viscosity and the surface tension increased due to the addition of the polyelectrolyte gelatin. Gelatin and pullulan formed hydrogen bonds, and the intermolecular hydrogen bonds increased while the intramolecular hydrogen bond decreased, which resulted in better mechanical properties. The electrospun gelatin/pullulan nanofibers could mimic both the structure and the composition of the extracellular matrix, and thus could be applied in tissue engineering.
Composite materials were prepared by the hot pressing method using poplar seed fibers and polycaprolactone (PCL) as the raw materials to solve the problems related to the recycling of waste fibers. The effects of mass fraction of poplar seed fibers, the volume density, and thickness on the sound absorption performance of the resulting composite materials were studied. The sound absorption coefficient curves of the composite material were obtained by the acoustic impedance transfer function method. The sound absorption coefficient of the composite material that was prepared under the optimal process conditions was higher than 0.7, and the effective sound absorption frequency band was wide. According to the box counting dimension method, which is based on the fractal theory, the fractal dimensions of the composite materials were calculated while using the Matlab program. The relationships between the fractal dimensions and the volume densities, mass fractions of poplar seed fibers, and thicknesses of the composite materials were also analyzed. Subsequently, the quantitative relationship between the fractal dimension and the sound absorption property parameters of the composite material was established in order to provide a theoretical basis for the design of the sound absorption composite material.
Conventionally laminated spacer composites are extensively applied in many fields owing to their light weight. However, their impact resistance, interlaminar strength, and integrity are poor. In order to overcome these flaws, the zigzag-shaped 3D woven spacer composites were rationally designed. The zigzag-shaped 3D woven spacer fabrics with the basalt fiber filaments tows 400 tex (metric count of yarn) used as warp and weft yarns were fabricated on a common loom with low-cost processing. The zigzag-shaped 3D woven spacer composites were obtained using the VARTM (vacuum-assisted resin transfer molding) process. The three-point bending deformation and effects of damage in zigzag-shaped 3D woven spacer composites were studied both in experiment and using the finite element method (FEM). The bending properties of zigzag-shaped 3D woven spacer composites with different direction, different numbers of weaving cycle, and different heights were tested in experiments. In FEM simulation, the geometrical model was established to analyze the deformation and damage based on the 3D woven composite structure. Compared with data obtained from the experiments and FEM simulation, the results show good agreement and also prove the validity of the model. Based on the FEM results, the deformation, damage, and propagation of stress obtained from the model are very helpful in analyzing the failure mechanism of zigzag-shaped 3D woven composites. Furthermore, the results can significantly guide the fabrication process of real composite materials.
In order to make reasonable utilization of poplar seed fibers, their macromolecular structure, supramolecular structure and morphological structure were analyzed by means of a biological microscope, scanning electron microscope, Fourier transform infrared spectrometer and X-ray diffractometer, and the relationship between the structure of poplar seed fiber and its sound absorption performance was explored. The acoustic impedance transfer function method was used to test the sound absorption performance of poplar seed fiber, kapok fiber, cotton fiber, wool fiber and hemp fiber aggregates that could be used in the field of sound absorption. The results showed that the order of sound absorption properties of the five fiber aggregates was as follows: kapok fiber, poplar seed fiber, cotton fiber, wool fiber, hemp fiber. The special structure of poplar seed fiber meant it had excellent sound absorption performance in the entire tested frequency range. The poplar seed fiber aggregate had a wide sound absorption frequency band and the maximum sound absorption coefficient reached 0.84, which has high application value in the field of sound absorption.
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