Multi-walled carbon nanotubes (MWCNT) were covalently functionalized with poly(3-hydroxybutyrate-co-3hydroxyvalerate) (PHBV) chains, through esterification reaction. Thereunto, pristine MWCNT (P-MWCNT) were oxidized (MWCNT-COOH) and posteriorly reduced (MWCNT-OH). MWCNT-OH were used to produce MWCNT functionalized with PHBV chains (MWCNT-PHBV). All functionalized MWCNT were used to produce PHBV nanocomposites films with 0.5 wt% by solution casting. Functionalization was evaluated by Raman spectroscopy and thermogravimetry (TGA), and nanocomposites were characterized by X-Ray Diffraction and contact angle measurements. Results showed that functionalization with PHBV chains was successfully performed and that the polymer chains were attached to MWCNT surface, as expected.
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