The aim of the presented work was to compare the results of grain size distribution measurement by an innovative dynamometer method, developed by the authors, with results obtained by the pipette and hydrometer methods. Repeatability of results obtained in the dynamometer method was also determined. The content of three fractions with equivalent diameters <0.002 mm, 0.002–0.063 mm and 0.063–2.0 mm was measured. The results were compared using ordinary linear regression and additionally in the repeatability analysis by RMA (reduced major axis regression). It was found that the proposed dynamometer method is characterized by good result repeatability with no systematic errors when compared with the pipette method. The RMSE (root mean square error) value when referring to the pipette method calculated for the three fractions considered in total was 4.9096 and was lower than the analogous for the hydrometer method, which amounted to 5.4577. Values of determination coefficients in the comparison of dynamometer method and pipette method are within the range of 0.9681–0.9951 for the different fractions. It was found that slightly larger differences in relation to the pipette method occurred for the fractions <0.002 mm and 0.002–0.063 mm, and smaller for the fraction 0.063–2.0 mm. Similarly, greater differences between repetitions in the dynamometer method were observed for the fraction <0.002 mm, and smaller for the 0.063–2.0 mm fraction. Possible sources of errors in the dynamometer method were discussed, as were proposals for their reduction.
The dynamometer method of determining particle size distribution was developed several years ago. The principles of sample preparation for this method are based on those used in other sedimentation methods. With improvements in these procedures, an investigation of the effect on obtained particle size distribution results by removing organic matter using hydrogen peroxide was proposed. For this purpose, the particle size distributions were determined in 50 soil samples with varying organic matter content, before and after organic matter removal. A comparative analysis of the results, including calculation of the Euclidean distance, was performed on both groups. It was found that differences in the particle size distributions of the soils after the application of hydrogen peroxide were difficult to predict, and irregular in both magnitude and direction. However, in light soils, the process of organic matter removal caused an increase in the clay fraction at the expense of the silt fraction, which decreased. In soils with a higher initial clay fraction, there were decreases in the clay and sand fractions, while the silt fraction increased.
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