We have studied the superconducting properties of Nd(Ba1−xNdx)2Cu3O7−δ (Nd123, x≊0.1) single crystals grown by the traveling-solvent floating-zone method under 0.1% O2 in Ar atmosphere. An anomalous peak effect in the magnetization hysteresis (M–B) loop is observed in the Nd123 single crystals as well as in the Nd123 bulk crystals prepared by the oxygen-controlled melt growth (OCMG) method. The critical current density (Jc) of the Nd123 single crystals is 70 600 A/cm2 in 1.0 T at 77 K for the applied field perpendicular to the a-b plane. Uniform flux density distribution with the same shape as the sample is observed in the field perpendicular to the a-b plane by the magneto-optical flux-density observation. Finely dispersed white regions in the dark-field image due to Nd substitutions for Ba are observed in the Nd123 matrix by the transmission electron microscopy. The high Jc value of the Nd123 single crystals in the applied field is explained by the field-induced pinning centers caused by the Nd–Ba substitutions in the Nd123 matrix.
Highly flat, clean, and stable surfaces of as-prepared Nd1Ba2Cu3Oy (Nd123) single crystals have been studied using an ultrahigh vacuum scanning tunneling microscope/spectroscopy (UHV-STM/STS) system. The results of large area STM scans together with the results of STS measurements, magnetization loops measured at several temperatures below Tc, and critical current density measurements reveal the presence of a new magnetic flux pinning center in Nd123 single crystals prepared in a reduced oxygen partial pressure. This pinning center is more conductive on the surface than the matrix and has a size ranging from several to several tens of nanometers as seen by STM. Similar pinning center may be introduced to other high temperature superconductors to increase their critical current densities in an applied magnetic field.
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