Mechanical properties of a developmental high strength and high toughness SiC, Generation I SX, have been evaluated under a Department of Energy (DOE)/Oak Ridge National Laboratory (ORNL) subcontract. The mechanical properties determined included flexural strength, tensile strength, and fracture toughness at room and elevated temperatures. Stress rupture, dynamic fatigue and creep at elevated temperatures also have been evaluated. The strength limiting factors have been identified at room and elevated temperatures. The strength controlling mechanisms are discussed. The microstructure-mechanical property relationship has been established.
Indentation cracking under sharp-pointed indenters is analyzed using compliance-based, nonlinear, fracture mechanics. The stress intensity factor, K , in linear elastic fracture mechanics is well known to be proportional to the load, P; in this nonlinear analysis K is proportional to P3'4. The observed relation between indenter load-point displacement and crack length is based on similitude of crack lengths with load-point displacements as a strain-controlled fracture. The equations that relate load and a function of the crack length to the crack driving force, J, have been found for Vickers indentations. Analysis of the nonlinear load vs displacement assumes an equilibrium crack in the elastic material surrounding the indent. The hardness that describes the load vs load-point displacement during cracking is derived on a constant J line in load-displacement space. The crack length is shown experimentally to be proportional to the load-point displacement after crack initiation for several different indenters in ZnS. The measured loading curves are nonlinear and display crack initiation during loading. The K,, expressions found here are very similar to correlations that have been applied to indentation cracks.
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