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Silicon carbide-based, environment friendly, biomorphic ceramics have been fabricated by the pyrolysis and infiltration of natural wood (maple and mahogany) precursors. This technology provides an eco-friendly route to advanced ceramic materials. These Fractographic characterization indicates the failure origins to be pores and chipped pockets of silicon.

The surface-crack-in-flexure (SCF) method uses a Knoop indenter to create small, semielliptical surface precracks in beam specimens. Lateral cracks may interfere with the primary median crack and cause errors of up to 10% in determination of fracture toughness, particularly for materials for which the fracture toughness is ϳ3 MPa⅐m 1/2 or less. Although the residual-stress-damage zone is ground or polished away by hand by removing 4.5-5 times the indentation depth, this amount may not be sufficient to completely remove the lateral cracks in low-fracture-toughness materials. A series of tests were conducted on sintered alpha silicon carbide with different amounts of material removed after indentation. Once the lateral cracks were fully removed, the SCF results concurred with single-edged-precracked-beam and chevron-notchedbeam data collected in accordance with ASTM Designation C1421. A simple remedy for the SCF method is to examine the outer ground surface for remnants of lateral cracks before fracture and to remove more material if necessary.

The slow crack growth parameters of several transparent armor ceramics were measured as part of a program to lighten next generation spacecraft windows. Transparent magnesium aluminate (spinel, MgAl2O4) and AlON exhibit superior slow crack resistance relative to fused silica, which is the historical material of choice. For spinel, slow crack growth, strength, and fracture toughness are significantly influenced by the grain size, and alumina‐rich phases and porosity at the grain boundaries lead to intergranular fracture in coarse grain spinel. Functions describing the required mass for a desired window life imply that transparent ceramics can lighten window panes from a slow crack growth perspective.

This report presents the results obtained by the five U.S. participating laboratories in the Versailles Advanced Materials and Standards (VAMAS) round-robin for fracture toughness of advanced ceramics. Three test methods were used: indentation fracture, indentation strength, and single-edge pre-cracked beam. Two materials were tested: a gas-pressure sintered silicon nitride and a zirconia toughened alumina. Consistent results were obtained with the latter two test methods. Interpretation of fracture toughness in the zirconia alumina composite was complicated by R-curve and environmentally-assisted crack growth phenomena.

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A notched coupon geometry was evaluated as a method for tensile testing of 2D triaxial braid composites. Edge initiated shear failure has been observed in transverse tension tests using straight-sided coupons based on ASTM D3039. The notched coupon was designed to reduce the effects of edge initiated failure and produce the desired tensile failure. A limited set of tests were performed with partial pressurization of tubes to determine the transverse tensile strength in the absence of edge initiated failure. The transverse strength measured with the notched coupons was considerably higher than the straight-sided coupons, comparable to the tube results, and closer to the maximum possible strength based on maximum fiber strain. Further investigations of the effects of the observed biaxial stress state and stress concentrations in the notched geometry are needed.

The eutectie system Ni-