In this paper, porous anodic aluminum oxide (AAO) membrane was prepared with highly pure aluminum film in 0.3M oxalic acid under dc voltage of 40V at about 8°C by two-step anodization. The morphology of the specimens processed in different stages of two-step anodization was observed with a scanning electron microscope (SEM). The electrochemical behavior of the anodized aluminum after different stages of two-step anodization was studied by electrochemical impedance spectroscopy (EIS). Different equivalent circuits were established to fit EIS experiment data, based on morphologies and structures of AAO during processing. The electrical elements in the equivalent circuits were used to explain experimental parameters.
Sol-gel method is used for the formation of Pb0.499Sr0.499TiO3 (PST)thin films. The initial films were prepared with spin coating sol solution on silicon wafer and drying at room temperature and then heating coated dry sol film at 400°C for 10min. This process was repeated for 1-4 times to obtain 4 initial films with different thicknesses. The 4 initial films were annealed at 700°C for 2h to obtain PST ceramics films. The morphologies of the surface and cross-section of PST films were observed with a scanning electronic microscope (SEM). The phase structures of PST films were analyzed using X-ray diffraction meter (XRD). Experimental results show that PST film prepared by coating sol on silicon with different thicknesses can be high smooth,uniform and compact film.
In this paper, effect of oxygen partial pressure on formation of Fe2O3 nanostructure during Thermal Oxidation was studied. Fe2O3 nanostructure was formed by controlling oxidation conditions (Po2) and using the method of thermal oxidation. To begin with, a piece of pure iron in a ceramic crucible was put in the tube furnace (SYS-G-Z-13). Next the metallic Fe was oxidized at 500°C for 4 hours, under different oxygen partial pressure including pure argon (Po2 = 0atm), air Po2 = 0.21atm) and pure oxygen (Po2 = 1atm) to produce nanostructure, respectively. The surface morphology of the oxidized specimens was observed by SEM. The crystalline structure of the nanostructure was determined by transmission electron microscope. The experimental results show that the density of nanosheets increases with increasing oxygen partial pressure.
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