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Numerical simulations are used in this work to investigate aspects of microstructure and microseg-regation during rapid solidification of a Ni-based superalloy in a laser powder bed fusion additive manufacturing process. Thermal modeling by finite element analysis simulates the laser melt pool, with surface temperatures in agreement with in situ thermographic measurements on Inconel 625. Geometric and thermal features of the simulated melt pools are extracted and used in subsequent mesoscale simulations. Solidification in the melt pool is simulated on two length scales. For the multicomponent alloy Inconel 625, microsegregation between dendrite arms is calculated using the Scheil-Gulliver solidification model and DICTRA software. Phase-field simulations, using Ni–Nb as a binary analogue to Inconel 625, produced microstructures with primary cellular/dendritic arm spacings in agreement with measured spacings in experimentally observed microstructures and a lesser extent of microsegregation than predicted by DICTRA simulations. The composition profiles are used to compare thermodynamic driving forces for nucleation against experimentally observed precipitates identified by electron and X-ray diffraction analyses. Our analysis lists the precipitates that may form from FCC phase of enriched interdendritic compositions and compares these against experimentally observed phases from 1 h heat treatments at two temperatures: stress relief at 1143 K (870 °C) or homogenization at 1423 K (1150 °C).

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In this work, a finite element model is developed for predicting the thermo-mechanical response of Ti-6Al-4V during electron beam deposition. A three-dimensional thermo-elasto-plastic analysis is performed to model distortion and residual stress in the workpiece and experimental in situ temperature, and distortion measurements are performed during the deposition of a single-bead-wide, 16-layer-high wall built for model validation. Post-process blind hole–drilling residual stress measurements are also performed. Both the in situ distortion and post-process residual stress measurements suggest that stress relaxation occurs during the deposition of Ti-6Al-4V. A method of accounting for such stress relaxation in thermo-elasto-plastic simulations is proposed where both stress and plastic strain are reset to 0, when the temperature exceeds a prescribed stress relaxation temperature. Inverse simulation is used to determine the values of the absorption efficiency and the emissivity of electron beam–deposited, wire-fed Ti-6Al-4V, as well as the appropriate stress relaxation temperature.

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