While repair is mainly used to restore the original part geometry and properties, hybrid manufacturing aims to exploit the benefits of each respective manufacturing process regarding either processing itself or resulting part characteristics. Especially with the current implementation of additive manufacturing in the production of TiAl, turbine blades for both hybrid manufacturing and repair new opportunities are enabled. One main issue is the compatibility of the two or more material types involved, which either differ regarding composition or microstructure or both. In this study, a TNMTM-alloy (Ti-Nb-Mo) was manufactured by different processes (casting, forging, laser additive manufacturing) and identically heat-treated at 1290 °C. Chemical compositions, especially aluminum and oxygen contents, were measured, and the resulting microstructures were analyzed with Scanning Electron Microscopy (SEM) and High-energy X-ray diffraction (HEXRD). The properties were determined by hardness measurements and high-temperature compression tests. The comparison led to an overall assessment of the theoretical compatibility. Experiments to combine several processes were performed to evaluate the practical feasibility. Despite obvious differences in the final phase distribution caused by deviations in the chemical composition, the measured properties of the samples did not differ significantly. The feasibility of combining direct energy deposition (DED) with either casting or laser powder bed fusion (LPBF) was demonstrated by the successful build of the dense, crack-free hybrid material.
V-Si-B and Mo-Si-B alloys are currently the focus of materials research due to their excellent high temperature capabilities. To optimize the mechanical alloying (MA) process for these materials, we compare microstructures, morphology and particles size as well as hardness evolution during the milling process for the model alloys V-9Si-13B and Mo-9Si-8B. A variation of the rotational speed of the planetary ball mill and the type of grinding materials is therefore investigated. These modifications result in different impact energies during ball-powder-wall collisions, which are quantitatively described in this comparative study. Processing with tungsten carbide vials and balls provides slightly improved impact energies compared to vials and balls made of steel. However, contamination of the mechanically alloyed powders with flaked particles of tungsten carbide is unavoidable. In the case of using steel grinding materials, Fe contaminations are also detectable, which are solved in the V and Mo solid solution phases, respectively. Typical mechanisms that occur during the MA process such as fracturing and comminution are analyzed using the comminution rate K P . In both alloys, the welding processes are more pronounced compared to the fracturing processes.
Previous studies showed the technical feasibility of additive manufacturing (AM) of Mo-Si-B alloys using the laser powder bed fusion (L-PBF) process. The competitiveness of the properties of AM alloys was demonstrated by a comparison to literature data from conventionally processed Mo-Si-B materials. In addition to the excellent mechanical properties at ambient and elevated temperatures, the oxidation resistance in a wide temperature range is another decisive aspect for the potential use of AM Mo-Si-B alloys. The present work shows investigations on the cyclic oxidation performance of a eutectic AM Mo-16.5Si-7.5B alloy. Depending on the temperature (800 °C, 1100 °C, 1300 °C), the oxidation mechanisms are different, which is due to different reactions at the surface of the alloys accompanied with mass changes of samples. These mass changes can be explained on the basis of microstructural investigations. However, compared to a directionally solidified (DS) alloy, the AM alloy shows improved oxidation resistance.
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