In recent years, the interest in reusing recycled fibers as building materials has been growing as a consequence of their ability to reduce the production of waste and the use of virgin resources, taking advantage of the potential that fibrous materials may offer to improve thermal and acoustic comfort. Composite panels, made of 100% wool waste fibers and bound by means of either a chitosan solution and a gum Arabic solution, were tested and characterized in terms of acoustic and non-acoustic properties. Samples with a 5 cm thickness and different density values were made to investigate the influence of flow resistivity on the final performance. Experimental results demonstrated that the samples had thermal conductivity ranging between 0.049 and 0.060 W/(m K), well comparable to conventional building materials. Similarly, acoustic results were very promising, showing absorption coefficients that, for the given thickness, were generally higher than 0.5 from 500 Hz on, and higher than 0.9 from 1 kHz on. Finally, the effects of the non-acoustic properties and of the air gap behind the samples on the acoustic behavior were also analyzed, proving that the agreement with absorption values predicted by empirical models was also very good.
Electrospinning makes it possible to obtain solid fibers, in addition to core-shell fibers, using coextrusion. However, an exhaustive control of parameters allows the core-shell fibers from emulsion electrospinning to be obtained. The solvent in the outer surface tends to evaporate and the polymer density increases, moving the emulsion drops towards the center, which in turn promotes coalescence, thus creating the core. The aim of this work was to avoid coalescence and obtain a net of nanofibers entrapping oil microcapsules. We obtained an emulsion oil in water (O/W), with polyvinyl alcohol (W) and two essential oils (O), sage and thyme. An electrospinning process was used to place the microcapsules of oil inside a net of nanofibers. The electrospun veil was characterized by organoleptic testing, SEM microscopy, FTIR spectroscopy, DSC thermal analysis, and pressure tests. Organoleptic testing, FTIR spectroscopy, and DSC thermal analysis demonstrated the presence of the oil, which was retained in the spheres observed by SEM microscopy, while pressure tests revealed that the oil remained in a liquid state. Furthermore, we demonstrated a strong relationship between the emulsion size and the final microcapsules created, which are slightly larger due to the shell formation. The size of the emulsion determines whether the spheres will be independent or embedded in the nanofibers. Furthermore, the nanofiber diameter was considerably reduced compared to the nanofibers without the oil.
The hydrophilicity of fibers is directly related to the comfort of a fabric and represents one of the most important aspects of a textile. Therefore, polyester (PES) modification has focused on an increase in moisture content and a subsequent improvement of the user’s experience. Based on the glycerol hygroscopic properties, the main objective has been the enhancement of the hydrophilicity of polyester by glycerol treatments. Furthermore, microwave irradiation and alkaline treatment have been applied, in order to increase glycerol adhesion. Treated PES samples were characterized by performing moisture content, negative ion, water diffusion and water vapor resistance analyses. The effect of different treatment conditions such as bath ratio (1/10 or 1/15), temperature (40, 60 or 100 °C), time (2 or 5 min) and microwave radiation intensity (300 or 500 W) was evaluated. The moisture content of treated PES results indicated that by decreasing the bath ratio and increasing the time and temperature the moisture gain can reach almost 14%, which can be easily related to increases in the weight of the fiber. The treatment with alkali was done and led to the highest moisture increase. Treatment with 500 W microwave irradiation led to higher glycerol retention after rinsing. Different experimental conditions were applied to the glycerol-treated PES fabrics, and a clear improvement in moisture content was obtained increasing the comfort. The results were compared with the ones obtained for cotton and wool, where the moisture is higher than non treated PES.
<div data-canvas-width="583.1287199999997">The last few years natural dyes rose in value. Some synthetics dyes are proven to be environmentally harmful and can cause negative effects. Due to the eco awareness the natural dyes were again wildly used. Tea extracts from the Camellia sinensis plant were used. Tea has a large range of phytoconstituents and some can be transferred onto the cotton fabric. The optimal time and temperature to obtain as many phytoconstituents as possible had to be established. The aim of this study was to optimize the extraction process from tea so as to apply the maximum concentration of phytoconstituents onto the textile fibers and improve the cotton functionalization (Ultra violet protection for example) once it is dyed with the extract. Results demonstrate time and temperature had a great influence on the optimization of the tea extracts. We could conclude that after 2 hours the most polyphenols, hydrolysable tannins and condensed tannins are obtained and increasing the time didn’t add any value. The temperature was a really important factor because the polyphenols derived around 70 °C so both the extraction temperature and dyeing treatment should be below 70 °C. Wastewater were characterized in order to determine the phytoconstituents were in the cotton fibres.</div>
Natural dyes, obtained from plants, insects/animals, and minerals, are renewable and sustainable bioresource products with minimum environmental impact. However, there are still many issues to solve related to natural dyes; consequently, synthetic dyes are still wildly used. Natural dyes have a low affinity towards the substrate cotton, so a solution had to be found: mordants. Mordants can also be harmful to the environment, which is why bio-mordants are used. The mordant used in this paper is chitosan. Cotton is pre-mordanted using the pad dyeing method. By using the exhaustion method, the fabric was coloured with red Camellia sinensis (tea) extracts. The colour, absorption of polyphenols and tannins, and ultraviolet protection (UPF) were tested. A comparison study was carried out between the cotton fabric and the cotton padded with chitosan at two different concentrations. The results are impressive. Cotton pre-mordanted with chitosan can absorb more polyphenols and tannins than cotton itself, and the colour fastness and UPF, once the fabric is laundered, demonstrate there is some kind of bonding between the fibre, quitosan, and active compounds from tea. The UPF was also doubled by using chitosan and the reddish colour obtained by Camellia sinensis extracts were darker on the cotton fabric. The increase in UPF protection on mordanted fabrics is higher than the gap obtained by colour difference, which means there are active compounds that do not confer colour, but enhance UPF protection.
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