Cellulose is a natural linear chain homopolymer that is an abundant and common component in all plants. Partially pure depolymerized cellulose, known as microcrystalline cellulose (MCC), is synthesized by mineral acids hydrolysis from α-cellulose precursors obtained from fibrous plants such as jute. Virgin soft and hardwoods are used as the main source of cellulose for raw materials of MCC production. These can be replaced by jute fiber to a great extent as it is considered one of the most promising alternatives. A proximate analysis had been carried out to determine the percentage of cellulose, hemicellulose, fats, and lignin in cellulose by standard methods. The cellulose purity of BJRI Tossa Pat-8 (Robi-1) fiber is identified from FT-IR. The IR results of MCC analysis were indicated 3,337.40cm-1 for the moisture and 1656.45cm-1 for carboxyl groups. In thermogravimetry analysis, at the first phase, 20-95oC is associated with moisture release. The oxidation of Tossa Pat-8 (Robi-1) MCC occurred in the range of 200-400oC. The remaining 0.65% of inorganic materials ash, was obtained at 425oC. This study indicates the cost-effective isolation of MCC from Tossa Pat-8 (Robi-1) and that can be promisingly applicable in several fields such as coatings and membranes explosives, cellulose, textiles, adhesives, films, textiles, food and tobacco, films, pharmaceutical and cosmetics industry, which needs further research.
Etherification of jute fibre with butyl chloride was carried out at a temperature of 300C for a period of 2 hours in different solvents. Sodium hydroxide was selected as swelling agent for cheap and availability. Petroleum ether was used as a solvent in this research. The degree of substitution, the percent elongation, and bundle strength and moisture regain of the butyl substituted jute fibre was studied. It is observed that the bundle strength of the butyl substituted jute fibre decreases and percentage of moisture regain of the butyl substituted jute fibre decreases with the increases of substitution. The extensibility of the butyl substituted jute fibre increases up to about 10 times of its original value of 1% extension at break with the increase of substitution.
Activated Carbons (ACs) were prepared from jute stick charcoal by chemical activation using H2SO4 and H3PO4 ranging temperature from 3000C to 3500. The activated carbons and charcoal prepared from jute sticks were characterized by evaluating the surface chemistry, structural features and surface morphology. The properties of the carbons were characterized by Scanning Electron Microscope (SEM), Brunauer – Emmett-Teller (BET), X-Ray Diffraction (XRD) and the FT-IR method. The jute sticks were converted to activated carbons with the highest surface area (135–245m2/g) and largest mesopores volume (0.14–0.16 cm3/g). The FT-IR spectra exhibited that the pyrolysis of jute stick resulted in the release of aliphatic and O - containing functional groups by thermal effect. However, the release of functional groups is effect of chemical reaction in the ZnCl2, H3PO4, and H2SO4 activation process. A honeycomb carbon structure in activated carbon was formed as observed on SEM images. Although charcoal and activated carbon were prepared at 3000C to 3500, the activated carbon exhibited much lower Raman sensitivity due to the formation of condensed aromatic ring systems. Due to high surface area and high porous structure with abundance of functional groups, the activated carbon prepared from jute sticks charcoal absorbed molecules with much higher than those of other activated carbon.
Jute is one of the natural cellulosic textile materials. It has many advantageous properties similar to cotton. Jute fibre has potential to impart different functionality by different chemical finishing for its diversification. In this research, Water repellent jute fabrics have been prepared by treating Nova TTC (fluorocarbon compound) different ratio and to find out the best formulation recipe. Treating fabrics have been impaired with a water repellent characteristic and showing good rating result on jute fabric .This water repellent fabric was suitable of various jute products for diverse textile uses.
Different fabrics were prepared by plain weaving with the blended yarns made of etherified jute fibre in the ratio of 50:50 with cotton, rayon and polyester. The physical properties of fabrics from blended yarns have been compared with those of cotton fabrics made with the same calculation 30 tex yarns. The mechanical properties of these fabrics were determined to monitor their serviceability in practical use and to ensure their suitability as jute blended cotton and synthetic fabrics. The softness and handling characteristics presented by the blending length and flexible firmness of the blended fabrics were much more comparable to that of the cotton fabrics with the indented fabric structure. The strength properties of etherified jute blended fabrics showed that the durability and serviceability of these fabrics was not much less than that of cotton fabrics due to any stress and deformation during use. It has also been observed that the blending of etherified jute with cotton, rayon, polyester or any other flexible fiber improves the draping properties of the fabrics made from it and in actual use these fabrics have almost the same bright look and firmness of cotton fabrics.
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