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This paper illustrates the thermal energy conservation potential of the so-called heat integrated distillation column (HIDiC), which combines advantages of direct vapour recompression and diabatic operation at half of the normal column height. In a typical close boiling mixture separation, compared with a column utilising the usual vapour recompression scheme, HIDiC halved the consumption of exergy at approximately the same capital cost, indicating a strikingly short pay-off time. The complexities of integrating the heat transfer equipment in the stripping section with proven gas/liquid contacting devices, which may work adversely to practical implementation of HIDiC concept, are also addressed.

The crystallization of phenanthrene fiom toluene with carbon dioxide as the antisolvent gas is described. In the GAS process, a pressurized

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