Development of homogenous metal matrix nanocomposites with uniform distribution of nanoreinforcement, preserved matrix nanostructure features, and improved properties, was possible by means of innovative processing techniques. In this work, Al-SiC nanocomposites were synthesized by mechanical milling and consolidated through spark plasma sintering. Field Emission Scanning Electron Microscope (FE-SEM) with Energy Dispersive X-ray Spectroscopy (EDS) facility was used for the characterization of the extent of SiC particles’ distribution in the mechanically milled powders and spark plasma sintered samples. The change of the matrix crystallite size and lattice strain during milling and sintering was followed through X-ray diffraction (XRD). The density and hardness of the developed materials were evaluated as function of SiC content at fixed sintering conditions using a densimeter and a digital microhardness tester, respectively. It was found that milling for 24 h led to uniform distribution of SiC nanoreinforcement, reduced particle size and crystallite size of the aluminum matrix, and increased lattice strain. The presence and amount of SiC reinforcement enhanced the milling effect. The uniform distribution of SiC achieved by mechanical milling was maintained in sintered samples. Sintering led to the increase in the crystallite size of the aluminum matrix; however, it remained less than 100 nm in the composite containing 10 wt.% SiC. Density and hardness of sintered nanocomposites were reported and compared with those published in the literature.
Abstract:The low hardness and strength of aluminum, which limits its use in many industrial applications, could be increased through the addition of nanoparticles. However, the appropriate processing method and parameters should be carefully selected in order to achieve the desired improvement in properties. In this work, aluminum was reinforced with low weight fraction (1 wt.%) of SiC nanoparticles and consolidated through spark plasma sintering. The effect of processing parameters on the densification, microstructure, and properties of the processed material was investigated. Field Emission Scanning Electron Microscope (FE-SEM) equipped with Energy Dispersive X-ray Spectroscopy (EDS) facility was used to characterize the microstructure and analyze the reinforcement's distribution in sintered samples. Phases present were characterized through X-ray diffraction (XRD). A densimeter and a digital microhardness tester were used to measure the density and hardness, respectively. Compressive tests were performed using universal testing machine. A fully dense Al-1 wt.% SiC sample was obtained. Analysis of density and hardness values showed that the influence of applied pressure was more pronounced than heating rate while the influence of sintering temperature was more significant than sintering time. Within the range of parameters used, the highest values of the characterized properties were obtained at a sintering temperature of 600 °C, sintering time of 10 min, pressure of 50 MPa, and heating rate of 200 °C/min.
OPEN ACCESSMetals 2015, 5 71
Polymer nanocomposite coatings with low friction and high wear resistance are being developed to protect aluminium surfaces against wear and tear during dry and boundary lubrication. In the present study, pure and graphene nanoplatelets (GNPs) reinforced ultra-high molecular weight polyethylene (UHMWPE) nanocomposite coatings are deposited on aluminium thrust bearings. Each bearing makes an ROD contact with a metallic disc counterface to simulate the contact configuration in an actual bearing. A set of tests involving pure and reinforced UHMWPE coatings under dry and liquid contact lubrication is conducted. The wear test results reveal that UHMWPE/1 wt-% GNPs performs better than the reference sample significantly. It reduces the friction and wear of aluminium both in the dry and boundary lubrication conditions at different conditions. The 1 wt-% GNPs reinforcement increases the load-bearing capacity of UHMWPE by 440% in the presence of base oil.
Ultra-high molecular weight polyethylene nanocomposite coatings reinforced with 1 wt.% graphene nanoplatelets were deposited on aluminum substrates. Sliding wear tests with a pin-on-disc configuration were conducted at different temperatures (25oC, 75oC, 90oC, 115oC, and 125oC) to evaluate the wear behavior of the coating at elevated temperatures. The ultra-high molecular weight polyethylene/1 wt.% graphene nanoplatelets nanocomposite coating showed an outstanding performance by passing the wear test without failing even until temperatures of 115oC as compared to the pure ultra-high molecular weight polyethylene coating which failed at a much lower temperature of 75oC, indicating an improvement in the operating temperature range of ultra-high molecular weight polyethylene by at least 44%.
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