The effect of heat treatment conditions on the microstructure and phase composition of a low activated high temperature ferritic-martensitic EK 181 steel (Fe-12Cr-2W-V-Ta-Ba) is studied. Addi tional thermal cycling about the austenite-martensite phase transition temperature between quenching and tempering hinders the formation of fine interstitial phases, decreases the phase transformation induced hard ening intensity, retards the formation of a substructure with continuous misorientations, and decreases the brittle-ductile transition temperature.
In this work, we study the effect of high-temperature thermomechanical treatment (HTMT) with deformation in the austenite region on the microstructure, tensile properties, impact toughness, and fracture features of advanced low-activation 12% chromium ferritic-martensitic reactor steel EK-181. HTMT more significantly modifies the steel structural-phase state than the traditional heat treatment (THT). As a result of HTMT, the hierarchically organized structure of steel is refined. The forming grains and subgrains are elongated in the rolling direction and flattened in the rolling plane (so-called pancake structure) and have a high density of dislocations pinned by stable nanosized particles of the MX type. This microstructure provides a simultaneous increase, relative to THT, in the yield strength and impact toughness of steel EK-181 and does not practically change its ductile-brittle transition temperature. The most important reasons for the increase in impact toughness are a decrease in the effective grain size of steel (martensite blocks and ferrite grains) and the appearance of a crack-arrester type delamination perpendicular to the main crack propagation direction. This causes branching of the main crack and an increase in the absorbed impact energy.
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