The normal-state charge transport is studied systematically in high-quality single crystals of BaFe2(As1−xPx)2 (0 ≤ x ≤ 0.71). By substituting isovalent P for As, the spin-density-wave (SDW) state is suppressed and the dome-shaped superconducting phase (Tc 31 K) appears. Near the SDW end point (x ≈ 0.3), we observe striking linear temperature (T ) dependence of resistivity in a wide T -range, and remarkable low-T enhancement of Hall coefficient magnitude from the carrier number estimates. We also find that the magnetoresistance apparently violates the Kohler's rule and is well scaled by the Hall angle ΘH as ∆ρxx/ρxx ∝ tan 2 ΘH . These non-Fermi liquid transport anomalies cannot be attributed to the simple multiband effects. These results capture universal features of correlated electron systems in the presence of strong antiferromagnetic fluctuations.
Advanced synchrotron radiation focusing down to a size of 300 nm has been used to visualize nanoscale phase separation in the K 0.8 Fe 1.6 Se 2 superconducting system using scanning nanofocus single-crystal X-ray diffraction. The results show an intrinsic phase separation in K 0.8 Fe 1.6 Se 2 single crystals at T< 520 K, revealing coexistence of i) a magnetic phase characterized by an expanded lattice with superstructures due to Fe vacancy ordering and ii) a non-magnetic phase with an in-plane compressed lattice. The spatial distribution of the two phases at 300 K shows a frustrated or arrested nature of the phase separation. The space-resolved imaging of the phase separation permitted us to provide a direct evidence of nanophase domains smaller than 300 nm and different micrometer-sized regions with percolating magnetic or nonmagnetic domains forming a multiscale complex network of the two phases.
High-density bulk materials of a newly discovered 40K intermetallic MgB2 superconductor were prepared by high pressure sintering. Superconducting transition with the onset temperature of 39K was confirmed by both magnetic and resistive measurements. Magnetization versus field (M-H) curve shows the behavior of a typical Type II superconductor and the lower critical field Hc1(0) estimated from M-H curve is 0.032T. The bulk sample shows good connection between grains and critical current density Jc estimated from the magnetization hysteresis using sample size was 2x10 4 A/cm 2 at 20K and 1T. Upper critical field Hc2(0) determined by extrapolating the onset of resistive transition and assuming a dirty limit is 18T
Superconductivity at about 8 K was observed in the metal-rich Li-Pd-B ternary system. Structural, microstructural, electrical, and magnetic investigations for various compositions proved that the Li2Pd3B compound, which has an antiperovskite cubic structure composed of distorted Pd6B octahedrons, is responsible for the superconductivity. This is the first observation of superconductivity in metal-rich ternary borides containing alkaline metal and Pd as a late transition metal. The compound prepared by arc melting has a high density and is relatively stable in the air. The upper critical fields H(c2)(0) estimated by linear extrapolation and the Werthamer-Helfand-Hohenberg theory are 6.2 and 4.8 T, respectively.
We report high-sensitivity microwave measurements of the in-plane penetration depth λ ab and quasiparticle scattering rate 1/τ in several single crystals of hole-doped Fe-based superconductor Ba1−xKxFe2As2 (x ≈ 0.55). While power-law temperature dependence of λ ab with the power ∼ 2 is found in crystals with large 1/τ , we observe exponential temperature dependence of superfluid density consistent with the existence of fully opened two gaps in the cleanest crystal we studied. The difference may be a consequence of different level of disorder inherent in the crystals. We also find a linear relation between the low-temperature scattering rate and the density of quasiparticles, which shows a clear contrast to the case of d-wave cuprate superconductors with nodes in the gap. These results demonstrate intrinsically nodeless order parameters in the Fe-arsenides. The discovery of high-T c superconductivity in Fepnictides [1] has attracted tremendous interests both experimentally and theoretically. The 'mother' materials have antiferromagnetic spin-density-wave order [2] and the superconductivity appears by doping charge carriers, either electrons or holes. Such carrier doping induced superconductivity resembles high-T c cuprates, but one of the most significant differences is the multiband electronic structure having electron and hole pockets in the Fe-based superconductors. Unconventional superconducting pairings, most notably the sign-reversing s ± state, have been suggested by several theories [3] featuring the importance of the nesting between the hole and electron bands. This is also in sharp contrast to other multiband superconductors such as MgB 2 , where the coupling between the different bands is very weak. Thus the most crucial is to clarify the novel multiband nature of superconductivity in this new class of materials.
Temperature dependent single-crystal x-ray diffraction (XRD) in transmission mode probing the bulk of the newly discovered K 0.8 Fe 1.6 Se 2 superconductor (T c = 31.8 K) using synchrotron radiation is reported. A clear evidence of intrinsic phase separation at 520 K between two competing phases, (i) a first majority magnetic phase with a ThCr 2 Si 2 -type tetragonal lattice modulated by the iron 5 × 5 vacancy ordering and (ii) a minority non-magnetic phase having an in-plane compressed lattice volume and a 2 × 2 weak superstructure, is reported. The XRD peaks due to the Fe vacancy 5 × 5 ordering in the majority phase disappear by increasing the temperature at 580 K, well above phase separation temperature confirming the order-disorder phase transition. The intrinsic phase separation at 520K between a competing first magnetic phase and a second non-magnetic phase in the normal phase both having lattice superstructures (that imply different Fermi surface topology reconstruction and charge density) is assigned to a lattice-electronic instability of the K 0.8 Fe 1.6 Se 2 system typical of a system tuned at a Lifshitz critical point of an electronic topological transition that gives a multi-gaps superconductor tuned a shape resonance. *
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