The purpose of this study was to evaluate the bond strength of metallic orthodontic brackets to feldspathic ceramic with different etching times, bonding materials and with or without silane application. Cylinders of feldspathic ceramic were etched with 10% hydrofluoric acid for 20 or 60 s. For each etching time, half of the cylinders received two layers of silane. Metallic brackets were bonded to the cylinders using Transbond XT (3M Unitek) or Fuji Ortho LC (GC). Light-activation was carried out with total exposure time of 40 s using UltraLume 5. Shear bond strength testing was performed after 24 h storage. Data were submitted to three-way ANOVA and Tukey's test (α=0.05). The adhesive remnant index (ARI) was used to evaluate the amount of adhesive remaining on the ceramic surface at ×8 magnification. Specimens etched for 60 s had significantly higher bond strength compared with 20 s. The application of silane was efficient in increasing the shear bond strength between ceramic and both fixed materials. Transbond XT showed significantly higher (p<0.05) bond strength than Fuji Orth LC. There was a predominance of ARI score 0 (clean ceramic failure surface) for all groups, with an increase in scores 1, 2 and 3 (adhesive material increasingly present on ceramic failure aspect) for the 60-s etching time. In conclusion, 60-s etching time, silane and Transbond XT improved significantly the shear bond strength of brackets to ceramic.
INTRODUCTION: At orthodontic treatment completion, knowledge about the effects of adhesive remnant removal on enamel is paramount. OBJECTIVE: This study aimed at assessing the effect of different adhesive remnant removal methods on enamel topography (ESI) and surface roughness (Ra) after bracket debonding and polishing. METHODS: A total of 50 human premolars were selected and divided into five groups according to the method used for adhesive remnant removal: high speed tungsten carbide bur (TCB), Sof-Lex discs (SL), adhesive removing plier (PL), ultrasound (US) and Fiberglass burs (FB). Metal brackets were bonded with Transbond XT, stored at 37oC for 24 hours before debonding with adhesive removing plier. Subsequently, removal methods were carried out followed by polishing with pumice paste. Qualitative and quantitative analyses were conducted with pre-bonding, post-debonding and post-polishing analyses. Results were submitted to statistical analysis with F test (ANOVA) and Tukey's (Ra) as well as with Kruskal-Wallis and Bonferroni tests (ESI) (P < 0.05). RESULTS: US Ra and ESI were significantly greater than TCB, SL, PL and FB. Polishing minimized Ra and ESI in the SL and FB groups. CONCLUSION: Adhesive remnant removal with SL and FB associated with polishing are recommended due to causing little damage to the enamel.
Objective This study aimed to evaluate in vitro the effects of whitening dentifrices on enamel color, the shear bond strength of orthodontic brackets and adhesive remnant index (ARI). Materials and Methods Eighty bovine teeth with brackets were randomly divided into four groups (n = 20): control group (GC)–water, test group 1 (GT1)–Colgate Total 12, test group 2 (GT2)–Curaprox Black Is White, and group test 3 (GT3)–Luminous White. All groups were submitted to brushing, simulating 12 months. The specimens were exposed to spectrophotometer color evaluation and to a shear strength test in a universal test machine using a 300 kN load with a crosshead speed of 0.5 mm/min. The ARI was evaluated with a stereoscopic magnifying glass. Statistical Analysis Nonparametric Kruskal–Wallis and Dunn’s tests were used for the color analysis, and Friedman and Nemenyi tests were used to compare the times in the variable. To compare the shear force between the groups, the data were evaluated by one-way analysis of variance and Tukey’s test, and ARI was analyzed using Fisher’s exact test, always with a significance level of 5%. Results In the color analysis, GT3 presented the greatest progression in whitening effect. GT1 had greater shear strength than GT3 did (p ≤ 0.05). For ARI, the score 1 was predominant in the GC and GT1. The GT2 and GT3 groups had scores of 3. Conclusion The whitening dentifrices promoted significant color change over the 12-month brushing time and may have interfered in the resistance to shear bond strength and ARI.
OBJECTIVE: The objective of this study was to assess, in vitro, the influence of bleaching gel and the use of desensitizing agent over bond strength of ceramic brackets bonded to bovine enamel. METHODS: One hundred bovine incisors were selected and randomly divided into five groups (n = 20): Group 1, control group (without bleaching); Group 2, bleached with 35% hydrogen peroxide; Group 3, bleached with 35% hydrogen peroxide (three applications, 15 minutes each) and desensitizing agent applied for 10 minutes; Group 4, bleached with 35% hydrogen peroxide for 40 minutes; Group 5, bleached with 35% hydrogen peroxide for 40 minutes with desensitizing agent applied for 10 minutes. Brackets were bonded 7 days after bleaching and submitted to shear bond strength test after 24 hours at a compression rate of 1 mm/minute. After fracture, the adhesive remnant index (ARI) was assessed under stereoscopic at 40 x magnification. Shear strength data (MPa) were submitted to one-way ANOVA and Tukey's test with significance level set at 5%. RESULTS: Group 5 (29.33 MPa) showed significantly higher bond strength than Group 1 (19.19 MPa), Group 2 (20.59 MPa) and Group 4 (23.25 MPa), but with no difference in comparison to Group 3. There was no significant difference among the other groups. The adhesive remnant index showed predominance of score 3, that is, all resin remained adhered to enamel for all groups. CONCLUSION: Bleaching with 35% hydrogen peroxide with calcium associated with desensitizing agent application produced higher bond strength values of brackets bonded to bovine enamel.
This study evaluated the effects of thermocycling and different light sources on the bond strength of metallic brackets to bovine tooth enamel using an adhesive resin. Bovine teeth were etched with 35% phosphoric acid gel for 20 s. After application of primer, metallic brackets were bonded to the buccal surface using Transbond XT, forming 8 groups (n=20), depending on the light source used for photoactivation (AccuCure 3000 argon laser - 20 s, Apollo 95E plasma arc - 12 s, UltraLume 5 LED - 40 s and XL2500 halogen light - 40 s) and experimental conditions without (Groups 1 to 4) or with thermocycling (Groups 5 to 8). Shear bond testing was carried out after 24 h of distilled water storage (Groups 1 to 4) or storage and thermocycling in distilled water (groups 5 to 8; 1,500 cycles - 5o/55oC). Data were subjected to two-way ANOVA and Tukey’s test (α=0.05). The Adhesive Remnant Index (ARI) was evaluated at ×8 magnification. No significant differences (p>0.05) in bond strength were found when the conditions without and with thermocycling were compared for any of the light sources. No significant differences (p>0.05) in bond strength were found among the light sources, irrespective of performing or not thermocycling. There was a predominance of ARI scores 1 in all groups. In conclusion, light sources and thermocycling had no influence on the bond strength of brackets to bovine enamel.
The aim of this study was to evaluate the effect of silanes, thermal cycling and acid etching on the shear bond strength (SBS) of metallic brackets to feldspathic ceramic. Feldspathic ceramic cylinders (Groups 1, 2, 5 and 6) were etched for 60 s with 10% hydrofluoric acid and Groups 3, 4, 7 and 8, without acid etching. Two layers of silane Clearfil Ceramic Primer (CCP, Groups 1 to 4) and two layers of RelyX Ceramic Primer (RCP, groups 5 to 8) were applied and dried for 60 s. Brackets were bonded to the cylinders with Transbond XT and light-activated for 40 s with Bluephase G2. All specimens were stored in deionized water at 37 °C for 24 h, and the specimens of groups 1, 3, 5 and 7 were submitted to 7,000 thermal cycles (5 °C/55 °C). After storage, the SBS test was performed at a crosshead speed of 1 mm/min. Data were subjected to three-way ANOVA and Tukey's post hoc test (α=0.05). The adhesive remnant index (ARI) was evaluated at 8x magnification. The SBS of CCP was significantly greater than of RCP (p<0.05), with or without thermal cycling. Thermal cycling significantly reduced the SBS (p<0.05). The groups submitted to acid etching showed significantly higher SBS than those without acid etching (p<0.05). In conclusion, thermal cycling reduced SBS for all groups. The best ceramic surface treatment for bracket bonding was achieved by acid etching and CCP silane. The ARI results showed predominance of score 0 for all groups.
ResumoIntrodução: Os elásticos corrente são acessórios indispensáveis no tratamento ortodôntico, e suas propriedades de grande interesse para o profissional, a fim de obter maior controle sobre os movimentos dos dentes. Objetivo: Avaliar a influência da marca comercial e comprimento da cadeia espaçadora de elásticos corrente na degradação de força. Material e método: Foram utilizadas ligaduras elásticas ortodônticas em cadeia, tipo curto, médio e longo das marcas: Rocky Mountain (RMO), TP e GAC. Os elásticos, contendo elos correspondentes a 12,5 mm, foram tensionados entre pinos de aço na máquina de ensaio universal Instron 4411 até 25 mm. O valor foi anotado. Após a aferição inicial da força, os elásticos foram fixados em placa de resina acrílica e mantidos distendidos a 25 mm. Foram inseridas em recipiente contendo água deionizada e mantidas em estufa a 37 °C. A leitura da força dos elásticos foi feita nos tempos de 24 horas, 48 horas, 7 dias, 14 dias, 21 dias e 28 dias. Os dados foram submetidos ao teste estatístico apropriado, com nível de significância de 5%. Resultado: Os elásticos TP apresentaram força significativamente maior em todos os períodos. Os elásticos GAC e RMO apresentaram forças estatisticamente semelhantes. Os elásticos TP cadeia curta e longa apresentaram força significativamente maior que os elásticos cadeia média. Para GAC e RMO os elásticos curto apresentaram força maior que os médios e este maior que os longos. Conclusão: A cadeia espaçadora e a marca comercial influenciaram nos resultados obtidos, reforçando a importância do conhecimento dos tipos de elástico.Descritores: Elastômeros; ortodontia; elasticidade. AbstractIntroduction: Elastic chains are indispensable accessories in orthodontic treatment. Changes in their properties are of great interest to professionals in order to gain greater control over tooth movements. Objective: Evaluate the influence of trademark and length of the spacer chain on force degradation of elastic. Material and method: We used the following elastic chain types: TP, Rocky Mountain (RMO) and GAC short, medium and long varieties. The elastics, which contained links corresponding to 12.5 mm, were tensioned between steel pins using Instron 4411 universal testing machine up to 25 mm. The value was recorded. After initial measurement of the force, the elastics were fixed on an acrylic resin plate and kept distended to 25 mm. They were inserted in a container with deionized water and kept in an incubator at 37º. The elastic force data was collected at time intervals of 24 hours, 48 hours, 7 days, 14 days, 21 days and 28 days. These records were subjected to an appropriate statistical test, with significance level of 5%. Result: TP elastics showed significantly higher force in all periods. RMO and GAC elastics showed similar elastic forces. Short and long TP elastics exhibited significantly higher strength than the average elastic chain. As regards GAC and RMO, short elastics showed higher than average force values, and higher values than the long type. Conclusion...
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